Quality detection method for Ruyi Zhenbao preparation

Abstract

The invention discloses a quality detection method related to a Ruyi Zhenbao preparation. The method comprises a qualitative identification method for banksia rose, dalbergia wood, clove, long pepper, safflower, cassia seeds and gallic acid and a content determination method for safflower yellow A in safflower, piperine in long pepper and cholic acid in bezoar. According to tests and research, when a sample is tested by using the identification method in the quality detection method provided in the invention, spots appear at positions on a chromatogram of the tested sample corresponding to positions where spots with same colors appear on a chromatogram of a contrast sample; negative controls produce no interference; the identification method is simple, feasible and remarkably characteristic. When the content determination method in the invention is used for determining the content of hydroxysafflower yellow A, piperine and cholic acid in the Ruyi Zhenbao preparation, it is proved thata good linear relation is obtained, that accuracy of tests of a recovery rate is high, that very good repeatability and stability are achieved and that accurate and strict control of quality of the the Ruyi Zhenbao preparation can be realized.

Description

technical field [0001] The invention belongs to a detection method for medicines, in particular to a quality detection method for Ruyi Bao preparations. Background technique [0002] Ruyi Treasure Preparation is a traditional Tibetan experience prescription. The prescription is derived from the "Supplement to Tibetan Medicine Formula" written by Desi Sangye Gyatso. It is the first choice for Tibetan medicine to treat various neurological diseases. Ruyi Zhenbao Pills are recorded in the national drug standard part of the local standard of Chinese patent medicine, standard number: WS 3 -BC-0314-95. The raw material medicine is composed of: mother of pearl 100g, safflower 100g, nutmeg 40g, parsley 40g, longan 30g, cinnamon 50g, buffalo horn 40g, artificial musk 2g, agarwood 100g, crab 50g, cardamom 40g, sandalwood 80g, 130g of myrobalan, 60g of frankincense, 50g of yellow sunflower, 2g of bezoar, 100g of travertine, 40g of clove, 130g of emblica, 40g of nigella seed, 80g of g...

AI Technical Summary

Problems solved by technology

[0003] Ruyi Treasure Maruhara standard (Standard number: WS 3 -BC-0314-95) The quality inspection method only has microscopic identification, no identification of medicinal materials and content determination items, which cannot fully reflect the quality of the drug, and the technical content is low, and the product quality cannot be effectively controlled.

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