Preparation method of algal polysaccharides toner
A technology of seaweed polysaccharides and skin care water, which is applied in the field of daily chemical products, can solve the problems of no patent application for polysaccharide skin care water, etc., and achieve the effect of strong activity, broad market prospects, and easy collection
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Embodiment 1
[0021] A preparation method of seaweed polysaccharide skin care water, comprising the steps of:
[0022] (1) Preparation of seaweed polysaccharide extract:
[0023] A. Put the cleaned centipede algae into an oven and bake at 40°C for 4 hours;
[0024] B, the dried centipede algae are pulverized with a universal pulverizer, and cross a 60-mesh sieve;
[0025] C. Add the pulverized centipede algae to double distilled water at a solid-to-liquid mass ratio of 1:40, place in a water bath at 100°C, and boil in water for 2 hours;
[0026] D. Centrifuge the water-bathed liquid with a high-speed centrifuge at 3000rmp / min, take the supernatant after 15 minutes, and use a rotary evaporator to rotate the supernatant to 1 / 4 of its original volume at 50°C;
[0027] E. Add 2 times the volume of absolute ethanol to the concentrated supernatant, and let it stand in a refrigerator at 4°C for 10 hours;
[0028] F. Centrifuge the ethanol-added supernatant at 3000rmp / min with a high-speed centr...
Embodiment 2
[0032] A preparation method of seaweed polysaccharide skin care water, comprising the steps of:
[0033] (1) Preparation of seaweed polysaccharide extract:
[0034] A. Put the cleaned centipede algae into an oven and bake at 60°C for 8 hours;
[0035] B, the dry centipede algae is pulverized with a universal pulverizer, crosses 80 mesh sieves;
[0036] C. Add the pulverized centipede algae to double distilled water at a solid-to-liquid mass ratio of 1:60, place in a water bath at 100°C, and boil in water for 4 hours;
[0037] D. Use a high-speed centrifuge to centrifuge the liquid obtained in the water bath at 5000rmp / min, take the supernatant after 25 minutes, and use a rotary evaporator to rotate the obtained supernatant to 1 / 4 of its original volume at 70°C;
[0038] E. Add 4 times the volume of absolute ethanol to the concentrated supernatant, and let it stand in a refrigerator at 4°C for 14 hours;
[0039] F. Centrifuge the liquid obtained in step E again at 5000rmp / mi...
Embodiment 3
[0043] A preparation method of seaweed polysaccharide skin care water, characterized in that: comprising the steps of:
[0044] (1) Preparation of seaweed polysaccharide extract:
[0045] A. Put the cleaned centipede algae into an oven and bake at 50°C for 6 hours;
[0046] B, the dry centipede algae is pulverized with a universal pulverizer, crosses 70 mesh sieves;
[0047] C. Add the pulverized centipede algae into double distilled water at a solid-to-liquid mass ratio of 1:50, place in a water bath at 100°C, and boil in water for 3 hours;
[0048] D. Use a high-speed centrifuge to centrifuge the water-bathed liquid at 4000rmp / min, take the supernatant after 20 minutes, and use a rotary evaporator to rotate the supernatant at 60°C to 1 / 4 of its original volume;
[0049] E. Add 3 times the volume of absolute ethanol to the concentrated supernatant, and let it stand in a refrigerator at 4°C for 12 hours;
[0050] F. Centrifuge the liquid obtained in step E again at 4000rmp / ...
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