Efficient and energy-saving repairing agent
A high-efficiency energy-saving, repairing agent technology, applied in the field of lubricating grease and lubricating oil, can solve problems such as instability, delamination effect, and dispersion defects
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[0023] 1. Borated alcohol amides
[0024] (1) Synthesis of borated ethanolamide
[0025] Add 120g of ethanolamine and 40g of boric acid into a three-neck flask with nitrogen protection and jacket heating, heat and stir until the boric acid is completely dissolved, then heat to 90°C, and react for 8 hours. The obtained product is a light yellow transparent liquid. In water and polar solvents.
[0026] (2) Synthesis of borated triethanolamide
[0027] Add 120g of triethanolamine and 40g of boric acid into a three-neck flask with nitrogen protection, jacket heating and stirring, heat and stir until completely dissolved, then heat to 95°C, and react for 8 hours. The obtained product is light yellow and transparent Liquid, soluble in water and polar solvents.
[0028] (3) Synthesis of borated anthranilamide
[0029] Add 120g of o-aminophenol and 40g of boric acid into a three-necked flask with nitrogen protection, jacket heating and stirring, heat and stir until completely diss...
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