Preparation method for vegetable tannin dye liquor and application thereof to dyeing aspect of real silk fabric
A technology of plant tannin and dye liquor, applied in the field of textile dyes, can solve the problems of restricting the popularization and application of natural dyeing materials, low dyeing fastness of silk fabrics, and low utilization rate of resources, etc., and achieves good industrial promotion prospects, significant ecological significance, Improve the effect of environmental degradation
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Embodiment 1
[0053] Larch bark powder (purchased from Inner Mongolia Sengong Extract Products Co., Ltd., 100 mesh), glacial acetic acid, sodium carbonate and iron sulfate are all commercially available.
[0054] Preparation of larch tannin dye solution: Weigh 100 g of larch bark powder and add 800 ml of distilled water, stir evenly, shake and extract at 80° C. for two hours, filter the extract to obtain a larch dye solution.
[0055] Using the forestry industry standard LY / T1082-2008 of the People's Republic of China "Analysis and Test Method for Tannin Extract", ferrous tartrate-spectrophotometry, vanillin-hydrochloric acid method or n-butanol-hydrochloric acid method to determine the content of tannin in the dyeing liquor is about 7 ~14%.
[0056] dyeing:
[0057] (1) Take clean silk fabrics for whitening, add larch dyeing liquor at a liquor ratio of 1:50, dyeing temperature is 80°C, adjust the pH of the dyeing liquor to 5, 7, and 8 with glacial acetic acid and sodium carbonate, and dye...
Embodiment 2
[0060] Red bayberry bark powder: wash the bayberry bark, dry it until the moisture content is lower than 40%, put it in a forced air oven and bake it at 85°C for 90 minutes, and grind it to 60 mesh to get the red bayberry bark powder. Glacial acetic acid, sodium carbonate, alum and ferric chloride are all commercially available.
[0061] Preparation of bayberry tannin dyeing solution: Weigh 100 g of bayberry bark powder and add 1000 ml of 80% acetone solution, conduct ultrasonic extraction at 50°C for 60 minutes (min), filter the extract to obtain arbutus chinensis dyeing solution.
[0062] Using the People's Republic of China forestry industry standard LY / T1082-2008 "Analysis and Test Method for Tannin Extract", ferrous tartrate-spectrophotometry, vanillin-hydrochloric acid method or n-butanol-hydrochloric acid method to determine the tannin content of bayberry dyeing solution is about 16 ~24%.
[0063] dyeing:
[0064] (1) Take clean silk fabrics for whitening, add the abo...
Embodiment 3
[0068] Black wattle extract (purchased from Guangxi Wuming extract factory), glacial acetic acid, sodium carbonate, iron sulfate and titanium sulfate are all commercially available.
[0069] Preparation of black wattle tannin dye solution: Weigh 10g black wattle extract and dissolve in 90ml distilled water, stir at 40°C for 15 minutes, let stand for 30 minutes, filter the obtained filtrate to be black wattle tannin dye solution.
[0070] Using the forestry industry standard LY / T1082-2008 of the People's Republic of China "Analysis and Test Method for Tannin Extract", ferrous tartrate-spectrophotometry, vanillin-hydrochloric acid method or n-butanol-hydrochloric acid method, the tannin content of black wattle dyeing liquor is about 28 ~41%.
[0071] dyeing:
[0072] (1) Take a clean silk fabric for whitening, add the above-mentioned black wattle tannin dye solution at a bath ratio of 1:50, dyeing temperature is 60°C, pH value is 6.5, and dyeing time is 90 minutes; then take ou...
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