System for reutilizing bromomethane by vacuum heating

A technology of vacuum heating and methyl bromide, applied in the field of chemical treatment, can solve the problems of high air tightness requirements of equipment, low purity of methyl bromide, poor desorption effect of methyl bromide, etc. Effect

Inactive Publication Date: 2012-11-28
中华人民共和国天津出入境检验检疫局
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Problems solved by technology

[0004] In the above patents, there are problems such as poor desorption effect of methyl bromide, low purity of methyl bromide recovered to steel cylinders and inconsistent purity each time, high operation requirements for condensation recovery to steel cylinders, high requirements for air tightness of equipment, and inconvenient replacement of activated carbon.

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  • System for reutilizing bromomethane by vacuum heating
  • System for reutilizing bromomethane by vacuum heating

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Embodiment Construction

[0018] In order to understand the present invention more clearly, describe the present invention in detail in conjunction with accompanying drawing and embodiment:

[0019] refer to figure 1 , the system includes: high temperature resistant, methyl bromide corrosion resistant pipeline 1, valve A2, valve B7, valve C12 and valve D14, methyl bromide concentration detector A3 and methyl bromide concentration detector B5, fumigation storehouse (or other fumigated closed facilities) 4 , vacuum pump 6, activated carbon or carbon fiber 8, temperature probe 9, heating chamber 10, carbon material filled column 11, circulation fan 13. Wherein, valve A2 and valve C12 are closed, and after fumigation treatment with methyl bromide in the fumigation storehouse (or airtight fumigation facility) 4, valve A2 and valve C12 are opened, and carbon material filled column valve D14 and valve B7 are opened at the same time, through circulation fan 13 And the pipeline 1 fully passes the methy...

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Abstract

The invention relates to a system for reutilizing bromomethane by vacuum heating, which comprises a heating cavity, a closed fumigation facility, a valve, a vacuum pump and pipelines, wherein a plurality of carbon material packed columns are arranged in the heating cavity, and the structure of each carbon material packed column is a cylinder with a cavity; the carbon material packed columns are connected in parallel and communicated; the upper communicating pipeline is led out of the upper part of the heating cavity and then connected with the vacuum pump, passes through the vacuum pump and is further connected to an upper pipeline interface of the closed fumigation facility; the lower communicating pipeline is led out of the lower part of the heating cavity and then connected with a circulating fan, passes through the circulating fan and is further connected to a lower pipeline interface of the closed fumigation facility; the carbon material packed columns adopt the vertical placement, thereby effectively solving the difficult problems of non-uniform distribution of activated carbon or carbon fibers, and difficulty in replacement of the activated carbon or the carbon fibers; the vacuum pump is adopted for vacuum-pumping of the carbon material packed columns, and then the bromomethane adsorbed in carbon material is heated for desorption, thereby improving the desorption effectand reducing the heating desorption temperature; and the bromomethane which is desorbed by vacuum heating can be directly discharged to the fumigation facility with goods to be fumigated, thereby reducing the reutilizing cost of the bromomethane.

Description

technical field [0001] The invention relates to the technical field of chemical treatment, in particular to a vacuum heating and recycling system for methyl bromide; the system is used for the recovery and reuse of methyl bromide after fumigation treatment of methyl bromide, and in particular, the method of vacuum heating is used to realize the recycling of methyl bromide. Background technique [0002] Methyl bromide is currently the most widely used fumigant in fumigation treatment in the world. Methyl bromide has the characteristics of widely killing insects, nematodes, germs and weeds, but because methyl bromide has a damaging effect on the ozone layer in the atmosphere, it was included in the controlled substances of the Amendment to the Montreal Protocol on Substances that Deplete the Ozone Layer in 1992 list. In order to reduce the damage to the ozone layer caused by the emission of methyl bromide after fumigation, it is necessary to study the technology for t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01M13/00B01D53/04
Inventor 黄庆林张瑞峰魏亚东程瑜
Owner 中华人民共和国天津出入境检验检疫局
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