Catalyst for decreasing cloud point of lube base oil and preparation method thereof
A lubricating oil base oil and catalyst technology, which is applied in the direction of molecular sieve catalysts, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the problems of limited conversion capacity of macromolecules and high cloud point of lubricating base oil products
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Embodiment 1
[0015] The preparation method and experimental operation steps of catalyst a are as follows:
[0016] Step ①: Based on the total weight of the mixed substance obtained in step ③, 5% of the ZSM-5 molecular sieve sample with a Si / Al molar ratio of 25.0 is used for 100% of the equivalent volume of adsorption with 0.2mol / L NaOH solution Stirring treatment at 80°C for 0.5h to obtain ZSM-5 microporous molecular sieve treated with alkali;
[0017] Step 2.: Based on the total weight of the mixed substance obtained in step 3., 15% cetyltrimethylammonium bromide template, 0.5% sodium aluminate and 30% sodium silicate and the rest water, stir evenly to obtain a gel;
[0018] Step ③: Add the alkali-treated microporous molecular sieve obtained in step ① into the gel obtained in step ②, stir evenly, and then use dilute H 2 SO 4 The solution adjusts the pH value of the synthesis system to 10.5;
[0019] Step ④: transfer the homogeneous colloid obtained in step ③ into a synthesis kettle, ...
Embodiment 2~4
[0023] According to the experimental procedure of Example 1 and the raw materials and operating conditions shown in Table 1, catalysts a, b, c, and d can be obtained.
[0024] Table 1 The parameters related to the preparation of catalysts a~d
[0025]
[0026]
Embodiment 5
[0028]The hydrogen-type composite molecular sieve obtained by ion exchange in Example 1 was prepared catalyst e according to the same aftertreatment method in Example 1 (by weight percentage of the catalyst, the content of alumina was 49%, and the content of Pt was 0.05%).
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