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Quality detection method for Jinhuaxiaocuo pills

A quality control method and technology for Xiaocuo pills, applied in the field of quality inspection of Jinhua Xiaocuo pills, can solve problems such as large limitations, difficulty in accurately controlling the quality of Jinhua Xiaocuo pills, etc., and achieve high quality standard level, characteristic spots Clear and simple results

Active Publication Date: 2010-06-16
KUNMING CHINESE MEDICINE FACTORY
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Problems solved by technology

The eleventh volume of "Drug Standards of the Ministry of Health of the People's Republic of China" promulgated the quality control standard of Jinhua Xiaocuo Pills (WS 3 -B-2169-96), but in the existing Jinhua Xiaocuo Pill quality control method issued by the Ministry of Health, there are only microscopic identification, 1 physical and chemical reaction and 1 thin-layer identification, which have great limitations and are difficult to accurately control Quality of Jinhua Xiaocuo Pills

Method used

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Effect test

Embodiment

[0019] The drug formula of Jinhua Xiaocuo Pill is composed of gardenia (stir-fried) 300g, mountain silver flower 300g, scutellaria baicalensis (stir-fried) 300g, rhubarb (wine-roasted) 300g, berberine 75g, bellflower 300g, mint 300g, phellodendron 75g, and licorice 150g.

[0020] Preparation method: the above nine flavors, gardenia, rhubarb, and coptis are crushed into coarse powder, and mixed; the remaining six flavors such as Scutellaria baicalensis are decocted twice for 1.5 hours each time, filtered, and the filtrates are combined, concentrated to a clear paste, spray-dried, The dry paste powder is added with gardenia and other shamisen coarse powders, mixed and pulverized into fine powders, sieved, pan-balled with 45-65% ethanol, coated with activated carbon, dried, and obtained.

[0021] Properties: This product is a black concentrated water pill with a yellowish-brown to brown center; bitter taste.

[0022] The quality detection method of Jinhuaxiaocuo pill of the present...

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Abstract

The invention relates to a quality detection method for Jinhuaxiaocuo pills (WS3-B-2169-96) in the eleventh volume of Drug Standard of Ministry of Public Health of the Peoples Republic of China (Chinese patent medicaments). Through the quality detection method for the Jinhuaxiaocuo pills, the quality control standard for the Jinhuaxiaocuo pills is improved, a method for detecting the content of a main ingredient in a preparation is established, physical and chemical reaction identification with poor specificity is eliminated, and thin layer chromatography identification methods for geniposide and berberine hydrochloride are improved to have the advantages of simplness and clear characteristic spots, thin layer chromatography identification methods for rhubarb, golden thread, amur corktree bark and baical skullcap root in the Jinhuaxiaocuo pills are increased, and the high quality standard level of the compound preparation is guaranteed.

Description

technical field [0001] The present invention relates to Jinhua Xiaocuo Pill (WS 3 -B-2169-96) quality testing method. Background technique [0002] The drug Jinhua Xiaocuo Pill in the eleventh volume of "Drug Standards of the Ministry of Health of the People's Republic of China" (prescription of traditional Chinese medicine) has the effects of clearing away heat and purging fire, detoxifying and reducing swelling, and is used for acne caused by excessive heat in the lung and stomach ( Acne), mouth sores, stomach fire and toothache, sore throat, red eyes, constipation, yellow and red urine embolism. The compound preparation is composed of 300g gardenia (stir-fried) of Chinese medicinal materials, 300g of mountain silver flower, 300g of scutellaria baicalensis (stir-fried), 300g of rhubarb (wine-roasted), 75g of berberine, 300g of bellflower, 300g of mint, 75g of Phellodendron cortex, and 150g of licorice. A total of 1000g was made. Among them, gardenia is the main drug in ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/756A61P17/10A61P1/02A61P11/04G01N30/36G01N30/90
Inventor 孙蓉朱敏
Owner KUNMING CHINESE MEDICINE FACTORY
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