Microcapsule targeting pesticide preparation for controlling dendrobium officinale insect damage
A Dendrobium officinale, pesticide preparation technology, applied in the field of pesticides, can solve the problems of Dendrobium candidum planting process hazards, inability to use, unstable water, etc., to reduce the number and frequency of pesticide application, improve environmental pressure, and reduce contact toxicity Effect
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Embodiment 1
[0023] Add urea and formaldehyde into a three-necked flask equipped with a thermometer and stirring device, the molar ratio is 1:2.0, after dissolving, add deionized water twice the weight of formaldehyde and urea, adjust the pH value to 8.5 with triethanolamine, and raise the temperature to 70 ℃, low-speed stirring reaction for 1 hour, the urea-formaldehyde resin prepolymer aqueous solution is obtained.
[0024] Dissolve 2.6g of 99% metaldehyde in 4.0g of benzene at normal temperature, add 5g of the above-mentioned urea-formaldehyde resin prepolymer aqueous solution while stirring, and add 7.5g of 5% sodium polyacrylate aqueous solution, and stir at 1500 rpm Form a stable O / W emulsion; reduce the speed to 800 rpm, add 1m hydrochloric acid in 5 batches within 60 minutes to adjust the pH of the system to 2.0, and polycondense for 1 hour; then increase the temperature to 45 degrees to solidify the capsule wall and add hydrogen after 1.5 hours Adjust the pH to 7.0 with sodium oxi...
Embodiment 2
[0026] Add urea and formaldehyde into a three-necked flask equipped with a thermometer and stirring device, the molar ratio is 1:2.0, after dissolving, add deionized water twice the weight of formaldehyde and urea, adjust the pH value to 8.5 with triethanolamine, and raise the temperature to 70 ℃, low-speed stirring reaction for 1 hour, the urea-formaldehyde resin prepolymer aqueous solution is obtained.
[0027] Dissolve 5.2g of 99% metaldehyde in 5.0g of benzene at normal temperature, add 7.5g of the above-mentioned urea-formaldehyde resin prepolymer aqueous solution while stirring, and add 10g of 5% sodium polyacrylate aqueous solution, and stir at 1500 rpm Form a stable O / W emulsion; reduce the speed to 800 rpm, add 1m hydrochloric acid in 5 batches within 60 minutes to adjust the pH of the system to 2.0, and polycondense for 1 hour; then raise the temperature to 45 degrees to solidify the capsule wall and add hydrogen after 2 hours Adjust the pH to 7.0 with sodium oxide, ...
Embodiment 3
[0029] Add urea and formaldehyde into a three-necked flask equipped with a thermometer and a stirring device, the molar ratio is 1:2.5, after dissolving, add deionized water twice the weight of formaldehyde and urea, adjust the pH value to 8.5 with triethanolamine, and raise the temperature to 70 ℃, low-speed stirring reaction for 1 hour, the urea-formaldehyde resin prepolymer aqueous solution is obtained.
[0030] Dissolve 10.4g of 99% metaldehyde in 6.0g of benzene at room temperature, add 15g of the above-mentioned urea-formaldehyde resin prepolymer aqueous solution while stirring, and add 20g of 5% sodium polyacrylate aqueous solution, and stir at 1500 rpm to form Stable O / W emulsion; reduce the speed to 800 rpm, add 1m hydrochloric acid in 5 batches within 60 minutes to adjust the pH of the system to 2.0, and polycondense for 1 hour; then increase the temperature to 45 degrees to solidify the capsule wall for 1.5 hours, then add hydroxide Adjust the pH to 7.0 with sodium,...
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