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Microcapsule targeting pesticide preparation for controlling dendrobium officinale insect damage

A Dendrobium officinale, pesticide preparation technology, applied in the field of pesticides, can solve the problems of Dendrobium candidum planting process hazards, inability to use, unstable water, etc., to reduce the number and frequency of pesticide application, improve environmental pressure, and reduce contact toxicity Effect

Inactive Publication Date: 2010-05-19
浙江森宇实业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, Dendrobium candidum has been artificially cultivated, but in the process of planting Dendrobium candidum, pests such as snails and slugs are often encountered to harm the shoots and thin stems of Dendrobium candidum, which will cause great harm to the planting process of Dendrobium candidum, seriously affecting this industry. Production of an endangered rare medicinal plant
[0004] With the development of science and technology, there are new requirements for the development of pesticides. Traditional pesticides are highly toxic, and there are many pesticide residues in plants, which will penetrate into soil, rivers or groundwater, affecting people's health, reducing soil quality, and causing Environmental pollution, so the formulation of pesticides is the direction of pesticide development; in addition, chemical pesticides also have the characteristics of decomposing under light, unstable to water, special odor, strong corrosion, etc., and the direct use effect is not ideal, or even unusable; With the continuous enhancement of people's awareness of safety, environment and ecological sustainable development, microcapsules have attracted people's attention, and it can overcome the above defects

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Add urea and formaldehyde into a three-necked flask equipped with a thermometer and stirring device, the molar ratio is 1:2.0, after dissolving, add deionized water twice the weight of formaldehyde and urea, adjust the pH value to 8.5 with triethanolamine, and raise the temperature to 70 ℃, low-speed stirring reaction for 1 hour, the urea-formaldehyde resin prepolymer aqueous solution is obtained.

[0024] Dissolve 2.6g of 99% metaldehyde in 4.0g of benzene at normal temperature, add 5g of the above-mentioned urea-formaldehyde resin prepolymer aqueous solution while stirring, and add 7.5g of 5% sodium polyacrylate aqueous solution, and stir at 1500 rpm Form a stable O / W emulsion; reduce the speed to 800 rpm, add 1m hydrochloric acid in 5 batches within 60 minutes to adjust the pH of the system to 2.0, and polycondense for 1 hour; then increase the temperature to 45 degrees to solidify the capsule wall and add hydrogen after 1.5 hours Adjust the pH to 7.0 with sodium oxi...

Embodiment 2

[0026] Add urea and formaldehyde into a three-necked flask equipped with a thermometer and stirring device, the molar ratio is 1:2.0, after dissolving, add deionized water twice the weight of formaldehyde and urea, adjust the pH value to 8.5 with triethanolamine, and raise the temperature to 70 ℃, low-speed stirring reaction for 1 hour, the urea-formaldehyde resin prepolymer aqueous solution is obtained.

[0027] Dissolve 5.2g of 99% metaldehyde in 5.0g of benzene at normal temperature, add 7.5g of the above-mentioned urea-formaldehyde resin prepolymer aqueous solution while stirring, and add 10g of 5% sodium polyacrylate aqueous solution, and stir at 1500 rpm Form a stable O / W emulsion; reduce the speed to 800 rpm, add 1m hydrochloric acid in 5 batches within 60 minutes to adjust the pH of the system to 2.0, and polycondense for 1 hour; then raise the temperature to 45 degrees to solidify the capsule wall and add hydrogen after 2 hours Adjust the pH to 7.0 with sodium oxide, ...

Embodiment 3

[0029] Add urea and formaldehyde into a three-necked flask equipped with a thermometer and a stirring device, the molar ratio is 1:2.5, after dissolving, add deionized water twice the weight of formaldehyde and urea, adjust the pH value to 8.5 with triethanolamine, and raise the temperature to 70 ℃, low-speed stirring reaction for 1 hour, the urea-formaldehyde resin prepolymer aqueous solution is obtained.

[0030] Dissolve 10.4g of 99% metaldehyde in 6.0g of benzene at room temperature, add 15g of the above-mentioned urea-formaldehyde resin prepolymer aqueous solution while stirring, and add 20g of 5% sodium polyacrylate aqueous solution, and stir at 1500 rpm to form Stable O / W emulsion; reduce the speed to 800 rpm, add 1m hydrochloric acid in 5 batches within 60 minutes to adjust the pH of the system to 2.0, and polycondense for 1 hour; then increase the temperature to 45 degrees to solidify the capsule wall for 1.5 hours, then add hydroxide Adjust the pH to 7.0 with sodium,...

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PUM

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Abstract

The invention relates to a preparation method of a microcapsule preparation having targeting effects on dendrobium officinale insect damage. The microcapsule comprises the following components in percentage by weight: 2 to 10 percent of methaldehyde, 1 to 10 percent of capsule core solvent, 0.3 to 1 percent of protective colloid, 1 to 5 percent of capsule wall material, 2 to 5 percent of wetting dispersant, 0.1 to 0.5 percent of viscosity modifier and the balance of water. Microcapsule suspending agent is prepared by taking methaldehyde as a capsule core by an interfacical polymerization method. Because methaldehyde has peculiar aroma which snails and land slugs like better, the microcapsule has targeting specificity; and the microcapsule preparation has the advantages of long pesticide effect, high insecticidal efficiency, simple preparation process, and the like.

Description

technical field [0001] The invention relates to the field of pesticides, in particular to a method for preparing a microcapsule targeted pesticide suspension for dendrobium officinale pests. Background technique [0002] Dendrobium candidum Wall.Ex Lindl is a traditional precious and rare Chinese medicinal material, which has unique effects such as nourishing the stomach and promoting body fluid, nourishing yin and clearing away heat. Before the 1990s, my country's medicinal Dendrobium was basically collected from wild resources in tropical and subtropical virgin forests. The huge market demand for a long time has caused excessive harvesting, resulting in wild Dendrobium being endangered. What's more serious is that due to indiscriminate digging and overharvesting, the natural environment on which wild dendrobium depends is facing devastating damage. [0003] At present, Dendrobium candidum has been artificially cultivated, but in the process of planting Dendrobium candidum...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N25/28A01N43/24A01N31/02A01P9/00
Inventor 俞巧仙叶智根周术涛雷志力
Owner 浙江森宇实业有限公司
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