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Method for detecting cholecytitis rehabilitation capsules

A technology of detection method and quality detection method, which is applied in the field of capsule detection, can solve the problems of unfavorable product control, poor controllability, and uncontrollable small flower Qingfengteng, and achieve the effect of facilitating monitoring and improving the level of quality monitoring

Active Publication Date: 2010-04-07
GUIZHOU BAILING GRP PARMACEUTIAL CO LTD
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AI Technical Summary

Problems solved by technology

Xiaohua Qingfengteng is the characteristic index component of Danyankang Capsules. In the existing quality standards of Danyankang Capsules, there is a lack of effective control methods for Xiaohua Qingfengteng, which makes the characteristic index ingredient Xiaohua Qingfengteng uncontrollable; and the existing Danyankang Capsules In the inspection method of Yankang Capsules, the preparation method of the test solution is not perfect, and the controllability is poor, which is not conducive to the control of the product by the manufacturer and the supervision department

Method used

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Effect test

Embodiment Construction

[0020] The detection method of this Danyankang capsule is calculated according to the weight. The Danyankang capsule is made of 200g of Lianchao, 200g of rhubarb, 200g of saxifrage, 200g of Xiaohuaqingfengteng, 200g of Fengweicao, 200g of scutellaria baicalensis, 200g of Phellodendron phellodendron, and Andrographis paniculata. 200g is made into 1000 capsules finished product; It is characterized in that, this detection method comprises the following steps:

[0021] Properties: This product is a capsule, the contents are brownish yellow to brown granules or powder, slightly gas, bitter taste;

[0022] Identification: (1) Take 6g of the content of this product, add 25ml of methanol, heat and reflux for 30 minutes, filter, evaporate the filtrate to dryness, add 1ml of absolute ethanol-chloroform (3:2) mixture to dissolve the residue, and use it as the test sample solution. Take another 1 g of the reference medicinal material of Lilynium chinensis, add 10 ml of methanol, heat an...

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Abstract

The invention discloses a method for detecting the quality of cholecytitis rehabilitation capsules. The method comprises the identification of glechoma, skullcap and sabia parviflora. The invention also discloses a detection method and a preparation method for the cholecytitis rehabilitation capsules. Based on the prior quality control, a TLC identification method for a main medicinal composition of the sabia parviflora of the cholecytitis rehabilitation capsules is increased, and a preparation method for sample solution in the detection method is modified. The method makes up for the defects in the prior quality control process, improves the level for monitoring the quality of products, and is favorable for monitoring the products by supervision and management departments.

Description

technical field [0001] The invention belongs to the technical field of pharmacy, and relates to a detection method of a capsule, in particular to a detection method of a capsule (common name or drug name Danyankang Capsule) for treating cholecystitis. Background technique [0002] Danyankang Capsule has the functions of clearing away heat and promoting dampness, removing stones and relieving pain, and is used for acute and chronic cholecystitis, cholangitis, cholelithiasis, and syndrome after gallbladder surgery caused by damp-heat accumulation in the liver and gallbladder. Xiaohua Qingfengteng is the characteristic index component of Danyankang Capsules. In the existing quality standards of Danyankang Capsules, there is a lack of effective control methods for Xiaohua Qingfengteng, which makes the characteristic index ingredient Xiaohua Qingfengteng uncontrollable; and the existing Danyankang Capsules In the inspection method of Yankang Capsules, the preparation method of th...

Claims

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Application Information

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IPC IPC(8): A61K36/756A61K9/48A61P1/16G01N30/02G01N30/90
Inventor 王晓冬郑周琴吴春玲
Owner GUIZHOU BAILING GRP PARMACEUTIAL CO LTD
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