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Method for flotation of potassium chloride from potassium salt mine

A technology for potassium chloride and potassium salt mines, applied in flotation, solid separation and other directions, can solve the problems of unfavorable flotation process promotion, complex production process, large total equipment investment, etc., and achieves good flotation effect and simple process. Stable, less circulating ore effect

Active Publication Date: 2009-07-08
YUNNAN CHEM RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This type of equipment is mainly adjusted according to experience in the adjustment of stirring speed and gas filling volume, which is not conducive to the promotion of flotation process, and makes the formed production process complicated, the total investment of equipment is relatively large, and the production cost is relatively high

Method used

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  • Method for flotation of potassium chloride from potassium salt mine

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] In the Chaerhan Saltfield Mine, the potassium content in the potash mine is 5.63%, and the magnesium content is 7.22%. Positive flotation process is adopted: the crushed ore particle size ranges from 3 to 8 mm, and fresh water is added for cold decomposition. Theoretical value of the fresh water addition amount of magnesium chloride, then adding fresh water cold decomposition, magnesium chloride is dissolved in water, the solid phase composition is potassium chloride and sodium chloride, and the flotation temperature is normal temperature. Introduce the ore pulp into the mineralization tank, add the saturated mother liquor of potassium chloride, sodium chloride and magnesium chloride, and add the positive flotation agent and mix thoroughly. The positive flotation agent is 1% octadecylamine hydrochloride, and the dosage is 2 %. The slurry concentration is 40%. The slurry is introduced into the flotation separation device. The flotation separation device is a micro-bubbl...

Embodiment 2

[0029] Laos solid potash mine, the potassium content in the potash mine is 8.4%, and the magnesium content is 5.13%. The positive flotation process is adopted, and the particle size of the crushed ore ranges from 3 to 8mm. The content of magnesium chloride in the raw ore was obtained by laboratory tests, and compared with the phase diagram of the quaternary water-salt system, the theoretical value of the amount of fresh water added just to dissolve magnesium chloride was calculated, and then fresh water was added for cold decomposition, magnesium chloride was dissolved in water, and the solid phase composition was potassium chloride and Sodium chloride, the flotation temperature is normal temperature. Introduce the ore pulp into the mineralization tank, add the saturated mother liquor of potassium chloride, sodium chloride and magnesium chloride, and add the positive flotation agent and mix thoroughly. The positive flotation agent is 1% octadecylamine hydrochloride, and the dos...

Embodiment 3

[0031]Laos solid potash mine, the potassium content of the potash mine is 8.1%, and the magnesium content is 4.83%. The positive flotation process is adopted, and the particle size of the crushed ore ranges from 3 to 8mm. The amount of fresh water added for cold decomposition is based on the sampling of the potash mine The content of magnesium chloride in the raw ore was obtained by laboratory tests, and compared with the phase diagram of the quaternary water-salt system, the theoretical value of the amount of fresh water added just to dissolve magnesium chloride was calculated, and then fresh water was added for cold decomposition, magnesium chloride was dissolved in water, and the solid phase composition was potassium chloride and Sodium chloride, the flotation temperature is normal temperature. Introduce the ore pulp into the mineralization tank, add the saturated mother liquor of potassium chloride, sodium chloride and magnesium chloride, and add the positive flotation agen...

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Abstract

The invention relates to a method for the floatation of potassium chloride in a sylvite mine, and a method for producing the product of chemical industry, in particular to a novel floatation method for extracting the potassium chloride from the sylvite mine. The method of the invention mainly comprises the following steps: a. the sylvite mine is pulverized and graded, the particle size of the pulverized mine rages from 3 to 8mm, and the pulverized mine is processed by the operation of cooling decomposition by being added with sweet water; b. mine slurry obtained in the step a is led into a mineralization slot and is added with the saturated mother solution of potassium chloride, sodium chloride and magnesium chloride as well as a positive floating agent; and the mine slurry, the saturated mother solution and the positive floating agent are completely mixed to control the concentration of the mine slurry to be from 20 to 40 percent; c. the mine slurry obtained in the step b is led into a flotation separation device to obtain the potassium chloride by the positive floatation; and d. particles fallen to the bottom of a flotation column are milltailings, particles which are discharged from the flotation column and are caused to float to the top end of the flotation column are potassium chloride particles, and the particles are collected to be concentrated, filtered and dried. The method has the advantages of simple and stable process, easier automatic control, favorable flotation effect, low agent consumption and production cost, etc.

Description

technical field [0001] The invention relates to a production method of chemical products, in particular to a new flotation method for extracting potassium chloride from potash ores. Background technique [0002] Potassium salt is a mineral resource in short supply in my country. Due to the lack of potassium resources, there is a large gap between the supply and demand of potassium resources in my country. The output of domestic salt lake potash fertilizer and other manufacturers only accounts for 30% of the demand, and the long-term dependence on imports is as high as 70%. [0003] There are mainly three kinds of raw materials for the production of potassium chloride fertilizer in my country. One is the chloride-type brine of the modern salt lake Chaerhan Salt Lake, which is mainly composed of carnallite and rock salt after drying the salt; It is carnallite and potassium halite; the third is seawater bittern as raw material. [0004] Potash mines mainly include potassium hal...

Claims

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Application Information

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IPC IPC(8): B03D1/00B03D1/08B03B1/00B03B1/04B03D1/02B03D1/01B03D1/14B03D103/10
Inventor 曾波王国栋郭会仙彭操刘文彪
Owner YUNNAN CHEM RES INST
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