Method for preparing high specific surface area granular activated carbon by physical activation process
A high specific surface area, granular activated carbon technology, applied in the field of material preparation, can solve problems such as low yield and failure to meet the application requirements of electric double layer capacitors, and achieve the effects of facilitating diffusion, shortening activation time, and improving the application range
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Embodiment 1
[0017] Example 1: Take 200g of coconut shell carbonized material after high-temperature carbonization, place it in a microwave radiation device, heat it to 900 ° C, feed water vapor, and its water vapor flow rate is 0.5L / min. After activating for 1.25 hours, a high specific surface area of activated carbon products. The yield is 42.2%, the iodine adsorption value is 1569.47mg / g, and the specific surface area is 2279m 2 / g, the pore volume is 1.212cm 3 / g.
Embodiment 2
[0018] Example 2: Take 150 g of coconut shell carbonized material after high-temperature carbonization, place it in a microwave radiation device, heat it to 850 ° C, and pass in CO 2 , where CO 2 The flow rate is 0.6L / min, and after 3 hours of activation, an activated carbon product with a high specific surface area is obtained. Its yield, iodine adsorption value, specific surface area and pore volume are 49.2%, 1456.37mg / g, 2203m 2 / g and 1.255cm 3 / g.
Embodiment 3
[0019] Example 3: Take 250 g of coconut shell carbonized material after high-temperature carbonization, place it in a microwave radiation device, heat it to 900 ° C, and feed water vapor and CO 2 A mixture of gases, where CO 2 The ratio of water vapor and water vapor is 3:1, the mixed gas flow rate is 0.8L / min, after 1 hour of activation, an activated carbon product with a high specific surface area is obtained. The yield is 50.6%, the iodine adsorption value is 1485.03mg / g, and the specific surface area is 2250m 2 / g, the pore volume is 1.157cm 3 / g.
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