Heat-resistant strippable micro-viscous pressure-sensitive adhesive film and preparation thereof
A sensitive adhesive film, micro-adhesive technology, applied in the field of heat-resistant peelable micro-adhesive pressure-sensitive adhesive film and its preparation, can solve the problem of inability to achieve direct peeling, etc., and achieve the effect of convenient operation
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Embodiment 1
[0054] In a three-neck flask equipped with a condenser, a stirrer, and a temperature needle, add 40 parts of 2-ethylhexyl acrylate (EHA), 20 parts of 2-ethylhexyl methacrylate (EHMA), and 17 parts of butyl acrylate. ester (BA), 16 parts methyl methacrylate (MMA), 7 parts hydroxyethyl acrylate (HEA), 150 parts toluene and 1 part initiator benzoyl peroxide. Stir and heat up to 80°C, stir and react at this temperature for 4 hours, then react at 90°C for 3 hours, and obtain a glue with a solid content of 35-40% after cooling.
[0055] Take 100 parts of the above glue solution, add 3 parts of toluene diisocyanate TDI, and stir at room temperature for half an hour to obtain a coating composition. Use a back coater to coat the coating composition on a 10 μm polyester film. Dry in an oven for 10 minutes, cover and roll with a release paper to obtain a peelable slightly viscous pressure-sensitive adhesive film of the present invention.
[0056] The above pressure-sensitive adhesive fi...
Embodiment 2
[0058] In a three-neck flask equipped with a condenser, a stirrer, and a temperature needle, add 40 parts of 2-ethylhexyl acrylate (EHA), 20 parts of 2-ethylhexyl methacrylate (EHMA), and 17 parts of butyl acrylate. Ester (BA), 16 parts of methyl methacrylate (MMA), 7 parts of hydroxyethyl acrylate (HEA), 150 parts of toluene and 1 part of initiator benzoyl peroxide are stirred and heated to 80 ° C, and stirred at this temperature React for 4 hours, then react at 90°C for 3 hours, and obtain a glue solution with a solid content of 35-40% after cooling.
[0059] Take 100 parts of the above glue solution, add 2 parts of toluene diisocyanate TDI, and stir at room temperature for half an hour to obtain a coating composition. Use a back coater to coat the coating composition on a 10 μm polyester film. Dry in the drying tunnel for 10 minutes, cover with release paper and roll up to obtain the peelable slightly viscous pressure-sensitive adhesive film of the present invention.
[00...
Embodiment 3
[0062] In a three-neck flask equipped with a condenser, a stirrer, and a temperature needle, add 40 parts of 2-ethylhexyl acrylate (EHA), 20 parts of 2-ethylhexyl methacrylate (EHMA), and 17 parts of butyl acrylate. Ester (BA), 16 parts of methyl methacrylate (MMA), 7 parts of hydroxyethyl acrylate (HEA), 150 parts of toluene and 1 part of initiator benzoyl peroxide are stirred and heated to 80 ° C, and stirred at this temperature React for 4 hours, then react at 90°C for 3 hours, and obtain a glue solution with a solid content of 35-40% after cooling.
[0063] Take 100 parts of the above glue solution, add 4 parts of toluene diisocyanate TDI, and stir at room temperature for half an hour to obtain a coating composition. Use a back coater to coat the coating composition on a 10 μm polyester film. Dry in the drying tunnel for 10 minutes, cover with release paper and roll up to obtain the peelable slightly viscous pressure-sensitive adhesive film of the present invention.
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