Condensation polymer type organic silicon die plastic and preparation technique of organic silicon resin for the same
A preparation process and silicone technology are applied in the field of preparation technology of polycondensation-type silicone molding compounds and special silicone resins, which can solve the problems of high thermal shrinkage, poor adhesion, and low softening point, and improve the environment. , the effect of reducing the reaction speed and improving the compatibility
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Embodiment 1
[0024] a. Raw material composition ratio by mass
[0025] Monomethyltrichlorosilane Purity>99% 60 parts
[0026] Dimethyldichlorosilane 99.9% purity 60 parts
[0027] One-phenyltrichlorosilane Purity>99% 120 parts
[0028] Ester functional silicone coupling agent purity >99% 90 parts
[0029] b. After fully mixing the above-mentioned organosilicon monomers, add 800 parts of toluene, 1000 parts of water, and 360 parts of ethylene glycol butyl ether solvent, co-hydrolyze at a temperature of 10°C, wash with water, and add 400 parts of dihydroxydiol Phenylsilane is used as a modifier, 1.8 parts of cobalt naphthenate is used as a catalyst for polycondensation, and finally the product is obtained by desolvating under the condition of a vacuum of 1kpa, cooling and pressing into tablets.
[0030] The performance of the obtained product is suitable for molding plastics, with good heat resistance and arc resistance, but slightly higher thermal elasticity and larger expansion coeffici...
Embodiment 2
[0032] a. Raw material composition ratio by mass
[0033] Monomethyltrichlorosilane Purity>99% 120 parts
[0034] Dimethyldichlorosilane 99.9% purity 60 parts
[0035] One-phenyltrichlorosilane Purity>99% 180 parts
[0036] Diphenyldichlorosilane purity>99% 60 parts
[0037] Organosilicon monomer containing double bonds, purity > 99%, 40 parts
[0038] Acryloyl silicone macromonomer Purity>99% 160 parts
[0039] b. After fully mixing the above silicone monomers, add 1200 parts of toluene, 1800 parts of water, and 600 parts of methyl ethyl ketone solvent, co-hydrolyze at a temperature of 10°C, wash with water, and add 660 parts of bisphenol A modified silicone The oligomer is used as a modifier, and 6 parts of cobalt naphthenate is used as a catalyst for polycondensation, and finally the product is obtained by desolventizing under the condition of a vacuum of 1kpa, cooling and pressing into tablets.
[0040] The performance of the obtained product is quite good, but the cu...
Embodiment 3
[0042] a. Raw material composition ratio by mass
[0043] Monomethyltrichlorosilane Purity>99% 120 parts
[0044] Dimethyldichlorosilane 99.9% purity 60 parts
[0045] One-phenyltrichlorosilane Purity>99% 120 parts
[0046] Diphenyldichlorosilane purity>99% 60 parts
[0047] Ester functional silicone coupling agent purity >99% 100 parts
[0048]b. After fully mixing the above silicone monomers, add 800 parts of toluene, 1100 parts of water, and 500 parts of methyl ethyl ketone solvent, co-hydrolyze at a temperature of 10°C, wash with water, and add 460 parts of bisphenol A modified silicone The oligomer is used as a modifier, and 2.3 parts of cobalt naphthenate is used as a catalyst for polycondensation, and finally the product is obtained by desolventizing under the condition of a vacuum of 1kpa, cooling and pressing into tablets.
[0049] The obtained product has good performance and is suitable for making molding compounds, but it is slightly soft at room temperature.
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