Metallic pigment, pigment dispersion liquid, metallic pigment ink composition, and ink jet recording method
A technology of ink composition and pigment dispersion, which is applied in the field of metal pigments and pigment dispersions, can solve problems such as difficult to use, burden of necessary pressurized equipment, and limitations of printing media
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Embodiment 1
[0113] 1. Manufacture of aluminum pigment dispersion
[0114] (1) A resin layer coating liquid having the following composition was formed into a uniform liquid film by spin coating on a PET film having a film thickness of 100 μm, and then dried to prepare a resin film layer.
[0115] (Resin layer coating solution)
[0116] Polyvinyl butyral resin (ェスレツクBL-10,
[0117] Sekisui Chemical Co., Ltd.) 3.0% by weight
[0118] Glycerin 2.0% by weight
[0119] IPA (isopropyl alcohol) balance
[0120] (2) Using the following apparatus, an aluminum vapor-deposited layer with a film thickness of 70 nm was formed on the above-mentioned resin layer.
[0121] Device: Co., Ltd. vacuum equipment, VE-1010 vacuum evaporation device
[0122](3) Using an ultrasonic disperser in IPA, the PET film having the laminate of the resin layer and the aluminum vapor-deposited layer formed by the above method was simultaneously peeled, miniaturized, and dispersed for 12 hours, and the cumulative time f...
Embodiment 2
[0154] The same operation as in Example 1 was carried out. However, the accumulation time of the dispersion treatment was extended from 12 hours to 18 hours to prepare ink composition 2 containing a metallic pigment. Table 1 shows the same evaluation results as in Example 1.
Embodiment 3
[0156] The same operation as in Example 1 was carried out. However, the accumulation time of the dispersion treatment was extended from 12 hours to 24 hours to prepare ink composition 3 containing a metallic pigment. Table 1 shows the same evaluation results as in Example 1.
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