Gale branch and leaves extraction disinfectant and its producing method
A production method and extract technology, which are applied in the field of botanical pesticides, can solve problems such as the ineffective utilization of resources, and achieve the effect of benefiting the environment and human food safety and reducing the pressure on the environment.
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Embodiment 1
[0030] Embodiment 1: drying waxberry branches and leaves to a moisture content of 10%, pulverizing them into 30 mesh powders, weighing 100kg of pulverized objects; using 300kg of methanol, extracting at a temperature of 50°C for 12h in a reflux extraction kettle, and obtaining after centrifugation Extraction; then carry out vacuum concentration until the concentrated solution is close to 100kg and end to obtain 100kg of extract for subsequent use.
[0031] According to the raw materials corresponding to Example 1 in Table 1 and the proportions by weight thereof, bactericide emulsifiable concentrate or bactericide microemulsion were respectively prepared. Specific instructions are given below:
[0032] Prepare fungicide emulsifiable concentrate according to Example 1 in Table 1: Add 80kg of the above-mentioned extract, 50kg of methanol, and 20kg of calcium laurate into the reaction kettle in turn, and stir evenly.
[0033] Example 1 in contrast table 1 prepares bactericide mic...
Embodiment 2
[0034] Embodiment 2: dry the branches and leaves of Myrica rubra to a water content of 8%, pulverize into 40 mesh powder, and weigh 80kg of pulverized matter; use 240kg of ethanol to extract at a temperature of 60°C, and the rest are the same as in Example 1, and finally concentrated Get 80kg of extract for subsequent use. Contrast the corresponding raw materials of Example 2 in Table 1 and the parts by weight thereof respectively with the same method as Example 1 (high-speed stirring temperature 50° C.) to prepare bactericide emulsifiable concentrate or microemulsion.
Embodiment 3
[0035] Embodiment 3: drying waxberry branches and leaves to a water content of 7%, pulverizing into 45 order powder, weighing 150kg pulverized matter; using ethyl acetate 450kg, extracting under 70 ℃ of temperature conditions, all the other are identical with embodiment 1 method, Concentrate at last to obtain 150kg of extract for subsequent use. Contrast the corresponding raw materials of Example 3 in Table 1 and the parts by weight thereof respectively with the same method as Example 1 (high-speed stirring temperature 55° C.) to prepare bactericide emulsifiable concentrate or microemulsion.
[0036] With the above three embodiments, the remaining five embodiments can be deduced according to the proportions in Table 1, and will not be listed one by one.
[0037] When preparing the extract, in addition to selecting the extraction solvent from factors such as cost and the performance of dissolving active ingredients, among the 8 examples listed in Table 1, examples 6, 7, and 8 a...
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