Method for preparing cellulose and silicon dioxide composite coloured fiber and coloured fiber made thereby
A silica and colored fiber technology, which is applied in the field of fiber production, can solve the problems of increasing energy consumption, manpower and cost, reducing the flame retardant effect of fibers, and affecting the flame retardant effect of fibers, so as to reduce environmental pollution and energy waste, Low cost, excellent flame retardant effect
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Embodiment 1
[0017] First, take sodium hexapolyphosphate or sodium tripolyphosphate and heat and dissolve it in 20g / l of dilute lye. Then, according to the coloring requirements of fiber production, mix the two evenly according to the ratio of sodium hexapolyphosphate to 2% of the weight of the color paste. After 2 hours, the colorant is prepared;
[0018] Secondly, cellulose cotton pulp is used to prepare cellulose xanthate by conventional short cellulose production method, and cellulose xanthogenate, silicon dioxide, sodium hydroxide and water are mixed uniformly to prepare a blended viscose liquid; The obtained blended viscose liquid is gradually matured by dissolving, filtering, and defoaming, and adding coloring agent in the dissolution to prepare a blended spinning dope, so that the weight content ratio of the prepared spinning dope is: α-fiber Element 5.0%, silicon dioxide 40% (for α-cellulose), sodium hydroxide 10.5%, colorant (calculated as solids) 3.4% (for α-cellulose), and moisture...
Embodiment 2
[0022] First, take sodium hexapolyphosphate or sodium tripolyphosphate and heat and dissolve it in 110g / l dilute lye. Then, according to the coloring requirements of fiber production, mix the two evenly according to the proportion of sodium tripolyphosphate accounting for 4% of the weight of the color paste. The colorant is prepared after 3 hours of mixing time;
[0023] Secondly, cellulose wood pulp is used to prepare cellulose xanthate by the conventional short cellulose production method, and cellulose xanthate, silicon dioxide, sodium hydroxide and water are mixed uniformly to prepare a blended viscose liquid; The obtained blended viscose liquid is gradually matured by dissolving, filtering, and defoaming, and the coloring agent is added before the viscose defoaming to prepare a blended spinning dope, so that the weight content ratio in the spinning dope is: α-fiber Element 8.0%, silica 60% (for α-cellulose), sodium hydroxide 10.2%, colorant (calculated as solids) 5.5% (for α-...
Embodiment 3
[0027] First, take sodium hexapolyphosphate or sodium tripolyphosphate and heat and dissolve it in 40g / l of dilute lye. Then, according to the coloring requirements of fiber production, mix the two evenly according to the ratio of sodium tripolyphosphate to 2.5% by weight of the color paste. After 2 hours, the colorant is prepared;
[0028] Secondly, cellulose cotton pulp is used to prepare cellulose xanthate by conventional short cellulose production method, and cellulose xanthogenate, silicon dioxide, sodium hydroxide and water are mixed uniformly to prepare a blended viscose liquid; The obtained blended viscose liquid is gradually matured by dissolving, filtering, and defoaming, and the coloring agent is added before the viscose defoaming to prepare a blended spinning dope, so that the weight content ratio in the spinning dope is: α-fiber Element 7.5%, silicon dioxide 20% (for α-cellulose), sodium hydroxide 10.5%, colorant (calculated as solids) 3.0% (for α-cellulose), and mois...
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