Vertical film flash distillation rectifying still for producing bio diesel fuel

A biodiesel and rectifying still technology, applied in flash evaporation, biological raw materials, biofuels, etc., can solve the problems of lower product yield, increase of distillation residue, prolonged residence time, etc., to improve heat utilization rate, reduce Grease loss, effect of reducing residence time

Inactive Publication Date: 2007-08-01
河南省商丘油脂化学厂
View PDF0 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

With this kind of horizontal rectification still, there are many and concentrated materials in the tower still, which not only affects the vaporization, but also prolongs the residence time of the materials in the still. Generally, the materials stay in the still for more than 30 minutes, which increases the conce

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Vertical film flash distillation rectifying still for producing bio diesel fuel

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0007] Structure of the present invention is as shown in accompanying drawing, is that the A3 steel plate of 10mm is welded a diameter 1200mm with thickness, the rectifying kettle 1 of high 4500mm, design pressure is 10kg / cm 2 , the production capacity is 3T / h. A tower-shaped thin-film evaporator 6 is designed in the rectification kettle 1, and the jacket 5 around the outer wall of the rectification kettle 1 and the thin-film evaporator 6 are heat-conducting oil, and the heat-conducting oil inlets 4 and 9 are located on the upper part of the jacket 5 , the heating area is 40m 2 , the heating temperature is 300°C; a flow limiter 2 is set on the top of the tower thin film evaporator 6, and a plurality of small holes 3 are arranged around the bottom of the flow limiter 2, and the upper part of the flow limiter 2 is connected to the crude methyl ester inlet 10; The ester steam outlet 11 is arranged on the top of the rectifying kettle 1 and connected to the condenser interface 12 ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention relates to a vertical film flash evaporation and distillation device for biodiesel production, mainly comprising rectifying still and film evaporator. The inside of annular tube around of rectifying still outer wall and inside of film evaporator are filled with heat conductive oil; the top of evaporator is equipped with a current limiter, all- around of bottom of current limiter is equipped with a plurality of eyelets, top of current limiter is connected with coarse methyl ester inlet; the coarse methyl ester enters into current limiter from inlet and flows out through said eyelets to heating wall of film evaporator and gasified instantly because of the high temperature of 300 Deg. C in the heating wall; gasified methyl ester enters into chiller and getting fine methyl ester. The invention is characterized in that it can greatly reduce the retention time for coarse methyl ester in rectifying still, reduces polymerzation; reduces fat consumption by over 10%, the continuous feed is possible and mass production is feasible; the heat carrier can be coal or electricity, heat availability ratio is increased by over 8%, the energy consumption is reduced and industrial benefit is increased.

Description

1. Technical field [0001] The invention relates to rectification equipment in biodiesel production. 2. Background technology [0002] At present, most countries in the world use horizontal rectification stills in rectification to produce biodiesel, and rely on tube preheaters and jackets to heat and vaporize. With this kind of horizontal rectification kettle, there are many and concentrated materials in the tower kettle, which not only affects the vaporization, but also prolongs the residence time of the materials in the kettle. Generally, the materials stay in the kettle for more than 30 minutes, which increases the concentration of unsaturated fatty acid formaldehyde. The generation of ester polymerization reaction increases the distillation raffinate like this, and the product yield decreases, and the general raffinate is about 15%. In addition, even if a vertical kettle is used, the inside of the kettle is empty and there is no flash device system. 3. Contents of the ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C10G3/00B01D3/06
CPCY02E50/13Y02E50/10Y02P30/20
Inventor 程方丁
Owner 河南省商丘油脂化学厂
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap