Powder coating composition, process for producing the same and coating film made from the same
A technology of powder coatings and manufacturing methods, applied in the direction of powder coatings, devices for coating liquid on surfaces, coatings, etc., can solve such problems that have not been developed
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Embodiment 1
[0081] Add aluminum powder for powder coating manufactured by Toyo Aluminum Co., Ltd. 665g (PCF 7640, D50=19μm: D50 is the average particle diameter, about 0.1g of the sample is dispersed in 5g of an aqueous solution of 0.5% Triton X (manufactured by UNION CARBIDE, surfactant), and water is used as the solvent. Dropped in Microtrac 9320X-200 manufactured by Honeywell, the value measured after ultrasonic dispersion (40W 10 seconds).), also added polyester resin powder 7000g (Teodur PE 785-900D50 manufactured by Kubo Kao Paint Co., Ltd. = about 49 μm), stirred and mixed for 10 minutes.
[0082] Then, as an adhesive adhesive, 105 g of terpane hydrogenated resin (Clearon P-105 manufactured by Yasuhara Chemical Co., Ltd., number average molecular weight 650, softening point 105° C.) was dissolved in 350 g of heptane (boiling point 98.4° C. ) to form a binder solution, then add it to the above-mentioned mixture of aluminum powder and resin powder, and stir for 20 minutes to become ...
Embodiment 2
[0084] 8.6 g of aluminum powder for powder coating (PCF1401, D50 = 60 μm) manufactured by Toyo Aluminum Co., Ltd. and 108.3 g of polyester resin powder (Teodur PE 785-900 D50 = about 49 μm manufactured by Kubo Paint Co., Ltd.) were mixed in 1 Mix well in a PP cup.
[0085] Adhesive adhesives were formed by dissolving 3.1 g of terpane hydrogenated resin (Clearon P-105 manufactured by Yasuhara Chemical Co., Ltd., number average molecular weight 650, softening point 105°C) in 31.3 g of heptane agent solution, and then added to the above-mentioned mixture of aluminum powder and resin powder, while fully mixing and stirring, while heating with a 40°C water bath from time to time, to evaporate the heptane. When the wet powder was almost dry, it was transferred to an eggplant-shaped flask and dried in a rotary evaporator at 40°C for 20 minutes under vacuum to completely evaporate the heptane. The obtained resin powder was passed through a 100 μm sieve to obtain 113.6 g of bonded alu...
Embodiment 3
[0087] Bonded aluminum was obtained in the same manner as in Example 2 using an aluminum powder for powder coating (PCF1440A, D50=34 μm) manufactured by Toyo Aluminum Co., Ltd.
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