Preparation method of polyolefin/montmorillonite nano-composite material
A technology of nano-composite materials and montmorillonite, which is applied in the field of preparation of polyolefin/montmorillonite nano-composite materials, can solve problems such as poor thermal stability, easy decomposition of quaternary ammonium salts, and degradation of material properties, and achieve good heat resistance , Simplified preparation process, low volatility effect
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Embodiment 1
[0028] Take 1 gram of 1-methyl-3-tetradecyl imidazole chloride, add 2 grams of Na-montmorillonite, and grind at room temperature for 5 minutes to obtain organic montmorillonite. Then, 98 grams of polyethylene were added and melt-blended to obtain a polyethylene / montmorillonite composite material. The XRD characterization results showed that the composite material was a polyethylene / montmorillonite nanocomposite material. The results are shown in Table 1.
Embodiment 2
[0030] Take 5 grams of 1-methyl-3-hexadecyl imidazole chloride, add 10 grams of Na-montmorillonite, and grind for 60 minutes to obtain organic montmorillonite. Then, add 90 grams of polyethylene, carry out melt blending, obtain polyethylene / montmorillonite nanocomposite material, the result is shown in attached table 1.
Embodiment 3
[0032] Get 3 grams of 1-methyl-3-(4-ethyl-hexadecyl) imidazole tetrafluoroborate, add 3 grams of mixed montmorillonite (the weight percentage of Na-montmorillonite and Ca-montmorillonite is 80 : 20), room temperature grinding 30 minutes, then, add 97 grams of polyethylene, carry out melt blending, obtain polyethylene / montmorillonite nanocomposite material. The results are shown in Table 1.
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