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Handheld dual thermal neutron detector and gamma-ray spectrometer

a dual-stage, gamma-ray spectrometer technology, applied in the direction of instruments, radiation measurement, measurement devices, etc., can solve the problems of poor phase homogeneity, and achieve the effect of improving purity and homogeneity, poor phase homogeneity

Active Publication Date: 2017-03-30
CONSOLIDATED NUCLEAR SECURITY +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The process yields high-purity, single-phase chalcopyrite crystals that enable efficient room temperature detection of neutrons and gamma rays, offering advantages in portability, sensitivity, and cost-effectiveness by integrating the neutron absorber within the semiconductor, reducing the need for external neutron absorbers and enhancing detection capabilities.

Problems solved by technology

For the lithium containing compounds, lithium reactivity is difficult to control, leading to poor phase homogeneity.

Method used

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  • Handheld dual thermal neutron detector and gamma-ray spectrometer
  • Handheld dual thermal neutron detector and gamma-ray spectrometer
  • Handheld dual thermal neutron detector and gamma-ray spectrometer

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exemplary embodiment 10

[0034]Referring specifically to FIG. 1, in the first exemplary embodiment 10, the Group VI elemental powder is added directly to the I-III alloy and heated to 700-900 degrees C. (depending on the group VI element) in a crucible 12. The reaction is allowed to proceed to completion and then cooled. Because the I-III compound is formed in an initial reaction step, the stoichiometry is defined as one mole for each element. Addition of the Group VI element for the final I-III-VI reaction has lower overall stoichiometric variability throughout the charge.

exemplary embodiment 20

[0035]Referring specifically to FIG. 2, in the second exemplary embodiment 20, the addition of the Group VI element into a single crucible is as with the first exemplary embodiment; however, the constituents are mixed at elevated temperature with constant crucible rotation at an angle 22, for example about 20 degrees. Rotation further promotes mixing during the synthesis to reduce phase variability.

exemplary embodiment 30

[0036]Referring specifically to FIG. 3, the third exemplary embodiment 30 involves vapor transport of the Group VI element 32. The previously prepared I-III compound is placed in one well of a crucible, while the Group VI element is placed in an adjacent well. As the mixture is heated to 700-900 degrees C., the Group VI element slowly vaporizes and is transported through thermal currents to the melted group I-III well. The reaction then occurs to form I-III-VI2. Vapor transport further slows the reaction to minimize overheating and promote a single phase synthetic charge.

[0037]It should be noted that the methods of the present invention are not limited to the synthesis of semiconductor materials. Doping with an activator (e.g., Group IV element) may be performed to create a scintillator material, for example.

[0038]Referring now specifically to FIG. 4, in one exemplary embodiment of the handheld dual thermal neutron detector and gamma-ray spectrometer 50 of the present disclosure, al...

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Abstract

A combined thermal neutron detector and gamma-ray spectrometer system, including: a first detection medium including a lithium chalcopyrite crystal operable for detecting neutrons; a gamma ray shielding material disposed adjacent to the first detection medium; a second detection medium including one of a doped metal halide, an elpasolite, and a high Z semiconductor scintillator crystal operable for detecting gamma rays; a neutron shielding material disposed adjacent to the second detection medium; and a photodetector coupled to the second detection medium also operable for detecting the gamma rays; wherein the first detection medium and the second detection medium do not overlap in an orthogonal plane to a radiation flux. Optionally, the first detection medium includes a 6LiInSe2 crystal. Optionally, the second detection medium includes a SrI2(Eu) scintillation crystal.

Description

CROSS-REFERENCE TO RELATED APPLICATION[0001]The present patent application / patent is a continuation-in-part (CIP) of co-pending U.S. patent application Ser. No. 13 / 658,591, filed on Oct. 23, 2012, and entitled “METHODS FOR SYNTHESIZING SEMICONDUCTOR QUALITY CHALCOPYRITE CRYSTALS FOR NONLINEAR OPTICAL AND RADIATION DETECTION APPLICATIONS AND THE LIKE,” the contents of which are incorporated in full by reference herein.STATEMENT REGARDING FEDERALLY SPONSORED RESEARCH OR DEVELOPMENT[0002]The U.S. Government has rights to the present disclosure pursuant to Contract No. ACO5-00OR22800 between the U.S. Department of Energy and Babcock and Wilcox Technical Services Y-12, LLC.FIELD OF THE DISCLOSURE[0003]The present disclosure relates generally to methods for synthesizing semiconductor quality chalcopyrite crystals for nonlinear optical and radiation detection applications and the like. More specifically, the present disclosure relates to methods for synthesizing a semiconductor detector of...

Claims

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Application Information

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Patent Type & Authority Applications(United States)
IPC IPC(8): G01T1/202G01T1/208G01T3/06
CPCG01T1/2023G01T1/208G01T3/06G01T1/202
Inventor STOWE, ASHLEY C.BURGER, ARNOLDBHATTACHARYA, PIJUSHTUPITSYN, YEVGENIY
Owner CONSOLIDATED NUCLEAR SECURITY
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