Catalyst in use for bromophenol
A catalyst and phenol technology, applied in the field of phenol bromination catalyst, can solve the problems of waste, environmental pollution, hydrogen bromide emission and environmental pollution, and achieve the effect of simple preparation device, good para-selectivity and stable catalyst
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Embodiment 1
[0021] Example 1: Put 20 g of multi-walled carbon nanotubes into 1 liter of nitric acid with a weight concentration of 50%, reflux at 50°C for 24 hours, cool, dilute the acidified carbon tubes with water, and adjust the pH value to 7.0 with 0.1M sodium hydroxide , then filtered, washed with water, and finally the acidified carbon tube was dried at 100° C. for 4 hours to make the water content less than 0.5%, and the catalyst acidified carbon tube could be prepared.
Embodiment 2
[0022] Embodiment 2: except changing the nitric acid that the weight concentration is 50% to the weight concentration is that the volume ratio of the nitric acid that is 63% and the sulfuric acid that the weight concentration is 98% is 1: 3, backflow 24 hours and change ultrasonic 5 hours, all the other and Process 1 is the same.
Embodiment 3
[0023] Embodiment 3: get the product 5 grams that embodiment 2 makes and 0.5 liters of Cr (NO 3 ) 3 After the saturated solution is mixed and stirred at room temperature for 8 hours, it is fully washed until neutral, filtered, and dried at 100°C for 4 hours to make the water content less than 0.5%, and then the acidified carbon tube containing chromium can be prepared.
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