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Quality control method for trauma treating Diedahongyao preparation

A quality control method and technology of red medicine, applied in the direction of testing pharmaceutical preparations, pharmaceutical formulas, antipyretics, etc., can solve problems such as the inability to effectively control the quality of Jieda red medicine preparations, affecting product production and ensuring quality.

Inactive Publication Date: 2006-11-08
JIANGXI HUIREN PHARMA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, existing quality control methods cannot effectively control the quality of Diedahongyao preparations, which will affect the production and quality assurance of products.

Method used

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  • Quality control method for trauma treating Diedahongyao preparation
  • Quality control method for trauma treating Diedahongyao preparation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0126] The quality control of embodiment 1 Diedahong pill (concentrated pill)

[0127] The quality control method of the present invention comprises the following steps:

[0128] The observation of character, the identification of content, the inspection of content, content determination is carried out to the composition that contains, therefore, the main steps of quality control method of the present invention are:

[0129] The observation of traits, the steps are:

[0130] [Properties] This product is a brownish-yellow to brown concentrated pill with a slightly pungent and bitter taste.

[0131] Content identification, the steps are:

[0132] [Identification] (1) Take 5g of this product, crush it, add 20ml of petroleum ether (60-90℃), ultrasonicate for 20 minutes, filter, evaporate the filtrate to dryness, add 1ml of petroleum ether (60-90℃) to dissolve the residue, As the test solution. Take 0.1 g of the reference drug of Angelica dahurica, add 10 ml of petroleum ether ...

Embodiment 2

[0143] The preparation of embodiment 2 Diedahong pills (concentrated pills)

[0144] Notoginseng 50.7g Safflower 11.8g Angelica 11.8g

[0145] Chuanxiong 11.8g Angelica dahurica 11.8g Wood beetle 11.8g

[0146] Preparation method of Diedahong pills (concentrated pills)

[0147] The above six flavors, Panax notoginseng, Chuanxiong, Angelica dahurica and Angelica are respectively crushed into fine powder and set aside. Safflower and ground beetle were reflux extracted with 60% ethanol three times, the first time was added 3.5 times, extracted for 6 hours, the second time was added 2.5 times, extracted for 4 hours, the third time was added 2 times, extracted for 2 hours, and the ethanol extracts were combined , filtered, the filtrate recovered ethanol and concentrated into a clear paste with a relative density of 1.05-1.07 (50°C), the clear paste was mixed with the above-mentioned fine powder and an appropriate amount of maltose, made into 1000 pills, dried, and polished to obt...

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Abstract

The present invention relates to quality control method for trauma treating Diedahongyao preparation. The quality control method includes thin layer chromatography process for material identification and spectrophotometric method for content measurement. The quality control method is precise, sensitive and stable, and can ensure the high and stable product quality.

Description

Technical field: [0001] The invention relates to a quality control method for traditional Chinese medicine preparations, in particular to a quality control method for Diedahong pill preparations. Background technique: [0002] "Dieda Red Tablets" is a product listed in Volume 20 of the Ministry of Health's Drug Standards for Traditional Chinese Medicine Prescriptions. For bruises, muscle and bone stasis, swelling and pain, rheumatic numbness. [0003] The monarch drug in the prescription, Panax notoginseng removes blood stasis to stop bleeding, activates blood to relieve pain, stops bleeding without leaving stasis, and is a wonderful product for regulating blood. In "Yu Catalpa Medicine Solution", "Sanqi and Ying stop bleeding, dredge the meridian and promote blood stasis, promote blood stasis and collect new blood. All... bruises, bloated, all blood stasis will be broken;... knife wounds, arrows, everything The new blood will all stop." The minister uses the soil beetle, ...

Claims

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Application Information

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IPC IPC(8): A61K36/8965A61K35/57A61P19/00A61P29/00G01N30/02G01N30/90G01N33/15
Inventor 李墅耿炤
Owner JIANGXI HUIREN PHARMA CO LTD
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