Combination of disinfectors and its applications used in aquiculture
A technology of aquaculture and composition, applied in the direction of application, biocide, animal repellent, etc., can solve problems such as unsatisfactory effect, secondary pollution, growth hazards of aquatic economic animals, etc., achieve good disinfection effect, increase oxygen concentration , Strong sterilization and disinfection effect
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Embodiment 1
[0023] At room temperature, chlorine gas is slowly passed into about 35% (weight percent) KOH solution, and stirred slowly until the chlorine gas is saturated and overflows. Add an appropriate amount of solid KOH to the reaction solution, stir until KOH is completely dissolved, cool with ice water, and filter to remove white crystals. The available chlorine content in the filtrate was determined by iodometric method.
[0024] Get above-mentioned filtrate, under vigorous stirring condition, slowly add the Fe(NO 3 ) 3 , control the temperature at about 20°C, stir and keep warm for about 1 hour, stop stirring, and filter. The filtrate is potassium ferrate solution. The potassium ferrate content of the solution was determined by the chromite method.
Embodiment 2
[0026] Take the potassium ferrate solution of known concentration prepared by the method in Example 1, add potassium hydroxide solid to saturation, cool down to about 15°C, fully separate out the crystals, and filter to obtain the crude purple-black potassium ferrate.
[0027] The crude product was dissolved in batches with a small amount of 3mol / L KOH solution, and transferred to a saturated KOH solution cooled with an appropriate amount of ice water for re-precipitation. After filtering, the filter cake was washed with benzene, ethanol and ether, and then vacuum-dried to obtain potassium ferrate crystals.
Embodiment 3
[0029] Get the potassium ferrate solution of known concentration prepared by the method of Example 1, add an appropriate amount of deionized water, the AEO-15 of solution total amount 15% (percentage by weight), stir evenly, measure the pH value of the solution, with It is advisable not to be lower than 9.0 (if less than 9.0, then adjust with 3mol / L KOH solution), and a potassium ferrate solution with a concentration of 0.1% (percentage by weight) is prepared.
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