Simple preparation method of Z-type heterojunction photocatalytic material
A technology of heterojunction and composite nanomaterials, which is applied in the field of photocatalysis, can solve the problems of narrow light absorption range, high recombination rate of photogenerated holes and electrons, and low photocatalytic efficiency, and achieve the effect of high safety and low cost
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Embodiment 1
[0027] The present invention provides a kind of composite nanomaterial, and its preparation method comprises the following steps:
[0028] 1) Disperse 6g of urea into ultrapure water to form a solution A with a concentration of 0.1mol / L;
[0029] 2) Rotary steam the solution A, and calcine it in a muffle furnace at 500 °C for 2 h to obtain g-C 3 N 4 powder A1;
[0030] 3) Disperse cupric chloride dihydrate into ultrapure water to form solution B with a solution of 0.1 mol / L;
[0031] 4) disperse sodium hydroxide into ultrapure water to form solution C with a concentration of 1mol / L;
[0032] 5) Disperse hydroxylamine hydrochloride in ultrapure water to form solution D with a concentration of 0.1mol / L
[0033] 6) Disperse A1 into ultrapure water to form suspension A2;
[0034] 7) Add 5 mL of B and 870 mg of sodium dodecyl sulfate to suspension A2, heat and keep the temperature at 35°C, stir for 40 min until the sodium dodecyl sulfate is completely dissolved, add 1.8 mL of ...
Embodiment 2
[0042] The present invention also uses the Cu prepared above 2 O@g-C 3 N 4 for photocatalytic reduction of CO 2 Methanol is produced, and water is oxidized to oxygen at the same time. The specific method is as follows:
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