Kapok extract as well as preparation method and application thereof
A kapok and extract technology, applied in the field of kapok extract and its preparation, can solve the problems of limited antioxidant capacity of kapok flavonoids and the like
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[0031] The application provides a preparation method of kapok extract, the preparation method of kapok extract comprises: using extractant to extract kapok, and collecting the liquid phase;
[0032] Wherein, the extractant includes the following components in parts by volume: 17-28 parts of betaine, 50-85 parts of glycerin and 0.4-9 parts of propylene glycol.
[0033] Specifically, the volume ratio of betaine, glycerol and propylene glycol is (17-28):(50-85):(0.4-9).
[0034] For example, the volume parts of betaine (chemical name N,N,N-trimethylglycine) can be 17 parts, 18 parts, 21 parts, 22 parts, 23 parts, 24 parts, 26 parts, 27 parts, 28 parts etc.
[0035] For example, the volume parts of glycerin can be 50 parts, 51 parts, 53 parts, 55 parts, 57 parts, 59 parts, 60 parts, 66 parts, 67 parts, 68 parts, 70 parts, 72 parts, 74 parts, 75 parts, 80, 81, 83, 84, 85 and so on.
[0036] For example, the volume parts of propylene glycol can be 0.4 parts, 0.5 parts, 1.2 parts,...
Embodiment 1
[0072] This embodiment provides a kind of kapok extract, which is mainly obtained through the following steps:
[0073] 1) The commercially available kapok is dried, pulverized, and passed through a 30-mesh sieve to obtain a powder. Take DES-TG and add water to configure 40% DES-TG aqueous solution to prepare extractant.
[0074] 2) Take 10g of kapok powder, add kapok according to the ratio of extractant to kapok powder of 1g:40ml, and perform high-voltage pulse extraction with a voltage of 600V and a pulse number of 80 times. Suction filtration is performed after the extraction is completed to obtain a kapok extract, which contains an extractant and an extract.
[0075] 3) The aluminum nitrate colorimetric method is used to detect the content of flavonoids in the kapok extract. Specifically, the detection method is as follows:
[0076] Take 2.4mL of kapok extract diluted to a certain multiple in a stoppered test tube, then add 5wt% NaNO 2 Solution 0.4mL, react after mixing...
Embodiment 2- Embodiment 5
[0078] Embodiment 2-Example 5 respectively provide a kind of kapok extract, please refer to Example 1, the difference between Example 2-Example 5 and Example 1 is that the extractant is different. In embodiment 2-embodiment 5, extractant adopts the following steps to make:
[0079] Mix betaine and ethanol, stir at room temperature until the solution is uniform, slowly add glycerin and propylene glycol, and then place the mixed solution in a nitrogen atmosphere at room temperature and magnetically stir for 8 hours. During the stirring process, the whole process is protected from light. Store at 0°C for 10h. Ethanol and water were removed by vacuum rotary evaporation to obtain the extractant, and the volume ratios of glycerol, propylene glycol and betaine are shown in Table 1.
[0080] All the other preparation methods and preparation techniques are the same as in Example 1.
[0081] Calculate the total flavonoid extraction rate according to the following formula:
[0082] To...
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