Preparation method of antioxidant based on AI-CQDs and AI-CNSs
An antioxidant, al-cnss technology, applied in the field of antioxidant preparation, can solve the problems of aging, cell damage and apoptosis, damage, etc., and achieve the effect of low cost, simple preparation method and environmental friendliness
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Embodiment 1
[0056] (1) Use high-purity Ti 3 AlC 2 Pressed tablets (purchased from Kaisen Ceramic Powder Co., about 1.5 cm in diameter and about 2 mm in thickness) were used as working electrodes, washed with absolute ethanol and deionized water for use.
[0057] (2) Use platinum wire as the counter electrode, carefully polish it and wash it with absolute ethanol and deionized water for use.
[0058] (3) Prepare electrolyte solution: prepare NaOH standard solution with a concentration of 0.1M as electrolyte.
[0059] (4) the above-mentioned working electrode (Ti 3 AlC 2 Tablet) and the counter electrode platinum wire were respectively fixed with electrode clamps, inserted into NaOH electrolyte solution, using CHI 660D electrochemical workstation, the technical parameters were constant potential method, the specific applied electrolysis voltage was 3V, and the reaction time was 6h.
[0060] (5) After the reaction is finished, the solution is taken out, and impurities are filtered using ...
Embodiment 2
[0065] (1) Use high-purity Ti 3 AlC 2 Pressed tablets (purchased from Kaisen Ceramic Powder Co., about 1.5 cm in diameter and about 2 mm in thickness) were used as working electrodes, washed with absolute ethanol and deionized water for use.
[0066] (2) Use platinum wire as the counter electrode, carefully polish it and wash it with absolute ethanol and deionized water for use.
[0067] (3) Prepare electrolyte solution: prepare NaOH standard solution with a concentration of 0.1M as electrolyte.
[0068] (4) the above-mentioned working electrode (Ti 3 AlC 2 Tablet) and the counter electrode platinum wire were respectively fixed with electrode clamps, inserted into the NaOH electrolyte solution, using CHI 660D electrochemical workstation, the technical parameters were constant potential method, the specific applied electrolysis voltage was 6V, and the reaction time was 6h.
[0069] (5) After the reaction is finished, the solution is taken out, and impurities are filtered us...
Embodiment 3
[0074] (1) Use high-purity Ti 3 AlC 2 Pressed tablets (purchased from Kaisen Ceramic Powder Co., about 1.5 cm in diameter and about 2 mm in thickness) were used as working electrodes, washed with absolute ethanol and deionized water for use.
[0075] (2) Use platinum wire as the counter electrode, carefully polish it and wash it with absolute ethanol and deionized water for use.
[0076] (3) Prepare electrolyte solution: prepare NaOH standard solution with a concentration of 0.1M as electrolyte.
[0077] (4) the above-mentioned working electrode (Ti 3 AlC 2 Tablet) and the counter electrode platinum wire were respectively fixed with electrode clamps, inserted into NaOH electrolyte solution, using CHI 660D electrochemical workstation, the technical parameters were constant potential method, the specific applied electrolysis voltage was 7.5V, and the reaction time was 6h.
[0078] (5) After the reaction is finished, the solution is taken out, and impurities are filtered usin...
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