Preparation method of chitosan fiber non-woven fabric applied to surface layer of paper diaper
A technology of chitosan fiber and non-woven fabrics, applied in wet spinning, stretch spinning, fiber chemical characteristics, etc., can solve the problems of poor prevention of diaper rash and other problems
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Embodiment 1
[0042] Method for preparing chitosan fiber nonwoven fabric applied to the surface of the diaper surface, including the following steps:
[0043] 1) Preparation of N-carboxyethyl chitosan
[0044] 20 g of a 20 g of an acetamin is 95% chitosan, 80 ml of acrylic acid and 1000 ml of distilled water to a three flask, and stirred and dissolved, and then the mixed liquid pH is 5.8-6.3, and magnetically stirred at 85 ° C temperature conditions for 8 h; reaction After the end, it was cooled to room temperature, precipitated with acetone, separated from centrifugation, and then dissolved in a small amount of water, precipitated again and centrifugally, and centrifugally, it was repeated three times, collecting the product, and placed the product in a culture dish In the case of filter paper, it is placed in a vacuum oven in a vacuum oven at a vacuum oven to react to constant weight, i.e., N-carboxyethyl chitosan;
[0045] Dehydrazine 95% chitosan feedstock, by viscosity method, it is measur...
Embodiment 2
[0060] Method for preparing chitosan fiber nonwoven fabric applied to the surface of the diaper surface, including the following steps:
[0061] 1) Preparation of N-carboxyethyl chitosan
[0062] 20 g of a 20 g of a deacetylate was 95% chitosan, 80 ml of acrylic acid and 1000 ml of distilled water to a three flask, and stirred and dissolved, and then the mixture pH of 5.8-6.3 was adjusted, and the magnetic force was stirred at 88 ° C temperature conditions; reaction After the end, it was cooled to room temperature, precipitated with acetone, separated from centrifugation, and then dissolved in a small amount of water, precipitated again and centrifugally, and centrifugally, it was repeated three times, collecting the product, and placed the product in a culture dish In the case of filter paper, it is placed in a vacuum oven in a vacuum oven at a vacuum oven to react to constant weight, i.e., N-carboxyethyl chitosan;
[0063] 2) Preparation of modified chitosan
[0064] N-carboxyet...
Embodiment 3
[0075] Method for preparing chitosan fiber nonwoven fabric applied to the surface of the diaper surface, including the following steps:
[0076] 1) Preparation of N-carboxyethyl chitosan
[0077] 20 g of a 20 g of a deacetyl is 95% chitosan, 80 ml of acrylic acid and 1000 mL of distilled water into a three flask, and stirred and dissolved, and then the mixed liquid pH is 5.8-6.3, and the magnetic force is stirred at 90 ° C temperature conditions for 5 h; reaction After the end, it was cooled to room temperature, precipitated with acetone, separated from centrifugation, and then dissolved in a small amount of water, precipitated again and centrifugally, and centrifugally, it was repeated three times, collecting the product, and placed the product in a culture dish In the case of filter paper, it is placed in a vacuum oven in a vacuum oven at a vacuum oven to react to constant weight, i.e., N-carboxyethyl chitosan;
[0078] 2) Preparation of modified chitosan
[0079] N-carboxyethyl...
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Abstract
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