N and P co-doped NF@NiMoO4 hollow nanowire composite material and preparation method and application thereof
A composite material, hollow nanotechnology, applied in the field of electrocatalysis, to achieve the effect of low cost, high HER catalytic activity, improved electrical conductivity and catalytic activity
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[0046] Below, the technical solution of the present invention will be described in detail through specific examples.
[0047] 1. Experimental method
[0048] 1. Characterization of samples
[0049] The compositional structure of the samples was characterized by using X-ray diffraction equipped with Cu Kα (λ = 0.154 nm) on a Smart lab SE diffractometer. The morphology of the samples was observed by scanning electron microscope and transmission electron microscope. X-ray photoelectron spectroscopy was used to characterize the composition and bonding state of the sample. All test results were calibrated for all element spectra using C1s (284.8eV) as the standard peak.
[0050] 2. Electrochemical performance test
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