Preparation method of ellagic acid microsphere and pomegranate leaf weight-losing black tea
A technology of pomegranate black tea and ellagic acid, which is applied in the field of food engineering, can solve the problems of low free state content, difficult utilization and instability of polymer pomegranate, etc., and achieves the effect of simple and convenient preparation method.
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Embodiment 1
[0031] β-cyclodextrin-ellagic acid microspheres pomegranate leaf slimming black tea, prepared by the following method:
[0032] S1. Dissolve 100g of β-CD in 4000ml of distilled water to form a saturated aqueous solution, then slowly drop in the ethanol solution of ellagic acid prepared from 25g of pomegranate peel ellagic acid and 200ml of ethanol, stir at room temperature on a magnetic stirrer for 2 hours, and cool to Put it in the refrigerator overnight at room temperature, and then freeze-dry it with a desktop vacuum freeze dryer for 48 hours. The obtained spongy substance is pulverized into β-cyclodextrin-ellagic acid microspheres;
[0033] S2. Collect the young leaves on the new shoots of the pomegranate tree, spread them in the withering tank and wither, the thickness of the spread is 1.5cm, 25°C, 75% relative humidity, flip once every 2h, wither for 8h, until the leaf surface rises Wrinkles, leaf color dark green, knead the withered leaves, kneading temperature is 25 ℃,...
Embodiment 2
[0039] Sodium alginate-chitosan-ellagic acid microspheres pomegranate leaf slimming black tea, prepared by the following method:
[0040] S1. Pipette 200mL 0.1mol / L hydroxylamine hydrochloride solution into a dry and clean 2500mL beaker, add 800mL 0.5g / L sodium alginate solution and shake well, then add 2g ellagic acid powder, shake quickly and place in Heat in a constant temperature water bath at 50°C for 1 hour to obtain the product. The product is filtered through a microporous membrane to obtain a filtrate. Add 50g of chitosan to the filtrate as a sustained-release agent, stir with a magnetic stirrer for 1 hour to form a uniform and stable suspension, then add 50mL of 2% glutaraldehyde solution, freeze at -80°C for 2h, and vacuum at -50°C Dry for 12 hours to obtain a spongy complex, which is ground and pulverized to form sodium alginate-chitosan-ellagic acid microspheres;
[0041] S2, collect the young leaves on the new shoot of pomegranate tree;
[0042] S3, spread the...
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