Degradable self-plugging-removal temporary plugging agent for reservoir drilling fluid, and preparation method thereof
A technology of drilling fluid and self-plugging removal, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve problems such as uncontrollable drilling fluid filtration effect, plugging rate, and permeability recovery value defects, etc., to achieve Improve blending performance, good degradability, and achieve the effect of degradation
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Embodiment 1
[0061] This example is to illustrate the degradable self-blocking temporary plugging agent prepared by the method of the present invention.
[0062] The preparation steps are as follows:
[0063] (1) Weigh 50 parts of lactide and 1 part of N-vinylpyrrolidone respectively into a polymerization tube, and add a certain amount of catalyst stannous octoate. Use an inert gas to remove oxygen; wait until the lactide crystals and polyvinylpyrrolidone are completely melted, shake it to make it fully mix with the catalyst, raise the temperature to 160°C and react for a certain period of time.
[0064] (2) Take it out after cooling down, purify it with acetone and dissolve it in deionized water. The precipitated polymer precipitate is the biodegradable temporary plugging material.
[0065] (3) Under vacuum and high pressure conditions, crush the biodegradable temporary plugging material into a powder state of 400 mesh, marked as S1.
[0066] In addition, the degradable self-blocking re...
Embodiment 2
[0068] This example is to illustrate the degradable self-blocking temporary plugging agent prepared by the method of the present invention.
[0069] Prepare biodegradable temporary plugging material according to the same method as in Example 1;
[0070] The difference is that the acid-soluble temporary plugging particles are a combination of magnesium carbonate, alumina and calcium lactate, the composition ratio of the components is 1:0.5:0.4, and the mass ratio of the biodegradable self-degrading plugging material to the acid-soluble temporary plugging material is 1: 1.
Embodiment 3
[0072] This example is to illustrate the degradable self-blocking temporary plugging agent prepared by the method of the present invention.
[0073] Prepare biodegradable temporary plugging material according to the same method as in Example 1;
[0074] The difference is that the acid-soluble temporary plugging particles are a combination of aluminum carbonate, aluminum oxide and calcium gluconate, the component ratio is 1:0.43:0.26, and the mass ratio of biodegradable self-degrading plugging materials to acid-soluble temporary plugging materials is 2 :3.
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