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A kind of fabric indigo dyeing method

A dyeing method and indigo technology, applied in the field of textile dyeing and finishing, can solve the problems such as the inability to reach the dark color of fiber penetration, the low dyeing rate and dye uptake rate, and the low fabric affinity, so as to save the foaming link and strengthen the penetration dyeing. effect, the effect of increasing the half-life

Active Publication Date: 2022-05-10
WUHAN TEXTILE UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Indigo is an indispensable vat dye in the denim textile industry. In the factory, it is mainly vat dyed through the traditional indigo reduction method. A large amount of sodium hydroxide is dissolved in an aqueous solution to form an alkaline environment, and then an appropriate amount of sodium hydrosulfite is added to stir and dissolve. Finally, indigo is added, and it is reduced to leuco indigo at a certain temperature to dye the fabric. This dyeing process not only consumes a large amount of chemicals, but also causes serious washing water pollution, water consumption and energy consumption. The subsequent wastewater discharge treatment is also at this stage. world problems
At the same time, due to the poor planarity of indigo water-soluble leuco molecules and low affinity to fabrics, resulting in low dyeing rate and dye uptake rate, poor penetrating ability, and difficult to dye dark colors, the current industry is based on indigo dyeing of cotton fibers. During the process, because the leuco indigo is easily oxidized, after the first dyeing, the oxidized leuco indigo is oxidized into indigo particles and adheres to the surface of the fiber, blocking the gaps in the fiber. The dyeing can not achieve the effect of deep color penetration of the fiber

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • A kind of fabric indigo dyeing method
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  • A kind of fabric indigo dyeing method

Examples

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Effect test

Embodiment 1

[0075] The embodiment of the present application provides a kind of fabric indigo dyeing method, comprises the following steps:

[0076] S1. Add 0.3 g of indigo to 100 mL of water, then add 2 g of Tween 80 and 3 g of absolute ethanol, and ultrasonically disperse to obtain a dispersion;

[0077] S2. Filter the dispersion with a positive pressure filter, and then ultrasonically disperse it again after the filtration to obtain an indigo suspension;

[0078] S3, add 0.4g hydrosulfite, 0.6g sodium hydroxide, foaming agent and stabilizer to 100mL indigo suspension under anaerobic environment, under 1200r / min, stir the foaming liquid for 3min to make it foam, and Foam is applied on pure cotton yarn, dyed, oxidized and fixed, and washed; wherein, the foaming agent concentration is 3g / L, and the foaming agent includes sodium lauryl sulfate, ten Sodium dialkylbenzenesulfonate and Tween 80, the stabilizer concentration is 1.2g / L, and the stabilizer includes citric acid, lauryl alcohol and...

Embodiment 2

[0081] The embodiment of the present application provides a kind of fabric indigo dyeing method, comprises the following steps:

[0082] S1. Add 0.3 g of indigo to 100 mL of water, then add 2.5 g of Tween 80 and 3.5 g of absolute ethanol, and ultrasonically disperse to obtain a dispersion;

[0083] S2. Filter the dispersion with a positive pressure filter, and then ultrasonically disperse it again after the filtration to obtain an indigo suspension;

[0084] S3, add 0.4g hydrosulfite, 0.6g sodium hydroxide, foaming agent and stabilizer to 100mL indigo suspension under anaerobic environment, under 1200r / min, stir the foaming liquid for 3min to make it foam, and The foam is applied at a grammage of 206g / m 2 On pure cotton cloth, dyed, oxidized, and washed; wherein, the concentration of the foaming agent is 3g / L, and the foaming agent includes sodium lauryl sulfate and lauryl sulfate with a mass ratio of 3:1:1 Sodium benzenesulfonate and Tween 80, the stabilizer concentration i...

Embodiment 3

[0087] The embodiment of the present application provides a kind of fabric indigo dyeing method, comprises the following steps:

[0088] S1. Add 0.3 g of indigo to 100 mL of water, then add 2 g of Tween 80 and 3 g of absolute ethanol, and ultrasonically disperse to obtain a dispersion;

[0089] S2. Filter the dispersion with a positive pressure filter, and then ultrasonically disperse it again after the filtration to obtain an indigo suspension;

[0090] S3, add 0.4g hydrosulfite, 0.6g sodium hydroxide, foaming agent and stabilizer to 100mL indigo suspension under anaerobic environment, under 1200r / min, stir the foaming liquid for 3min to make it foam, and The foam is applied on pure cotton yarn, dyed, oxidized and fixed, and washed; wherein, the concentration of the foaming agent is 3g / L, the foaming agent is sodium lauryl sulfate, and the concentration of the stabilizer is 1.2g / L, which is stable The agent is citric acid;

[0091] Among them, the ultrasonic dispersion in S...

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Abstract

The invention provides a fabric indigo dyeing method, comprising the following steps: adding indigo to water, then adding Tween 80 and absolute ethanol to obtain a dispersion liquid; filtering the dispersion liquid and ultrasonically dispersing again to obtain an indigo suspension; Add sodium lauryl sulfate, citric acid, hydrosulfite, and alkali to the indigo suspension under an oxygen environment to obtain a foaming liquid, stir to make it foam, apply the foam to the fabric, dye, and oxidize to fix the color. The fabric indigo dyeing method of the present invention uses Tween 80 and absolute ethanol to disperse the indigo, and then prepares the nano-blue suspension through an ultrasonic dispersion process, and uses hydrosulfite to reduce the indigo suspension under alkaline conditions in combination with an oxygen-free environment Form leuco indigo, combine with foam system, stir and foam, and carry out foam dyeing. The performance of foam dyeing is better in all aspects after the combination of ultrasonic pulverization and anaerobic environment. The dyed fabric is sweat-resistant, water-resistant, wear-resistant and breathable. Sex and K / S value apparent color depth are good.

Description

technical field [0001] The invention relates to the technical field of textile dyeing and finishing, in particular to a fabric indigo dyeing method. Background technique [0002] Indigo is an indispensable vat dye in the denim textile industry. In the factory, it is mainly vat dyed through the traditional indigo reduction method. A large amount of sodium hydroxide is dissolved in an aqueous solution to form an alkaline environment, and then an appropriate amount of sodium hydrosulfite is added to stir and dissolve. Finally, indigo is added, and it is reduced to leuco indigo at a certain temperature to dye the fabric. This dyeing process not only consumes a large amount of chemicals, but also causes serious washing water pollution, water consumption and energy consumption. The subsequent wastewater discharge treatment is also at this stage. world problems. At the same time, due to the poor planarity of indigo water-soluble leuco molecules and low affinity to fabrics, resulti...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06P1/22D06P1/673D06P1/96
CPCD06P1/228D06P1/6735D06P1/965D06P2001/0092
Inventor 易长海朱豆豆易红陈阳
Owner WUHAN TEXTILE UNIV
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