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ITO etching solution for TFT-LCD display screen and preparation method

A technology of etching solution and display screen, which is applied in the direction of chemical instruments and methods, surface etching composition, etc., can solve the problems of difficult control of etching precision, severe etching reaction, high cost of etching solution, etc., and achieve excellent anti-corrosion effect and excellent production process Simple and satisfying technical process and process requirements

Pending Publication Date: 2021-08-03
合肥中聚和成电子材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] In the prior art, CN201210206045.5 discloses the aqua regia system of nitric acid / hydrochloric acid, CN201110132527.6 discloses the hydrochloric acid / acetic acid system, CN201911163144.8 discloses the ferric chloride / hydrochloric acid system, and CN201610860973.1 discloses the sulfuric acid / nitric acid system , the content of the acid used is high, the etching reaction is violent, and it is difficult to control the etching precision. It is not suitable for the ITO film layer with a small thickness, and the cost of the etching solution is high. During the process, it needs to be continuously replenished to ensure the stability of the component content

Method used

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  • ITO etching solution for TFT-LCD display screen and preparation method
  • ITO etching solution for TFT-LCD display screen and preparation method
  • ITO etching solution for TFT-LCD display screen and preparation method

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Embodiment

[0027] An ITO etching solution for TFT-LCD display screen, comprising the following components by weight percentage: 14wt% sulfuric acid, 3wt% ammonium sulfate, 1wt% 2-mercaptoimidazole, 0.1% surfactant, 0.05 wt% % defoamer, balance water.

[0028] The etching object of the etching solution is ITO film, the etching time is 50s, and the etching temperature is 40℃; the etching results are as follows figure 1 As shown, the unilateral CD after etching is 0.0595um, and the slope angle of ITO is 33°; figure 2 Shown is the result of etching Mo, Al, and Cu by the etching solution, the etching time is 600s, the etching temperature is 40 °C, and the etching solution does not corrode the Mo, Al, and Cu metal layers; image 3 Shown is the result of etching the Cu glass sheet for 600 s with the etching solution, and no pitting is found.

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Abstract

The invention relates to the technical field of wet electronic chemicals, and discloses an ITO etching solution for a TFT-LCD display screen. The ITO etching solution comprises the following components by weight: 10%-20% of sulfuric acid, 1%-5% of an additive, 0.05%-0.5% of a surfactant, 0.01%-0.1% of a defoaming agent, and the balance of water, wherein the additive is a mixture of inorganic salt and organic matter. The etching solution disclosed by the invention takes sulfuric acid as a main component, the production process is simple, and the acid concentration is easy to control and detect on line; the surfactant is added and has low surface tension, no cloud point and strong wetting power, the surface tension of the ITO etching solution is effectively reduced, and the rate in the etching process is moderate; the defoaming agent can eliminate foam generated by the surfactant in the etching process, meets the high-precision processing requirement of ITO film etching, has no destructive effect on photoresist, well protects etching lines, and enables the pattern to be complete; and meanwhile, the adopted inorganic salt can regulate and control the gradient of the ITO inclined surface after etching, so that the requirements of customers can be better met.

Description

technical field [0001] The invention relates to the technical field of wet electronic chemicals, in particular to an ITO etching solution for a TFT-LCD display screen and a preparation method. Background technique [0002] TFT-LCD has high resolution and good image display effect, its energy consumption is low, cost is getting lower and lower, and image effect is getting better and better, thanks to the continuous innovation of basic chemical materials and cost reduction. In the production of TFT-LCD, the TFT structure plays a very important role in the display as the switch of the electrode, and the etching of the ITO film is the last process in the fabrication of the TFT pattern Array. After the ITO film is sputtered, a layer of photoresist is covered, the pattern is exposed and developed, the ITO film is etched with an etchant, and the photoresist is peeled off to form the desired pattern. In addition, with the development of the display industry, the production line pro...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K13/06
CPCC09K13/06
Inventor 许磊黄德新何烨谦
Owner 合肥中聚和成电子材料有限公司
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