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Water-based modified polyurethane dispersion, application thereof and hair conditioner prepared from the same

A technology of polyurethane dispersion and hair conditioner, which is applied in the field of water-based modified polyurethane dispersion and its use and the hair conditioner prepared by it, can solve the problems of unsatisfactory hair antistatic effect and the like, and achieve the maintenance of normal colony balance and no appearance. Influence and reduce the effect of dandruff

Active Publication Date: 2021-05-11
WANHUA CHEM GRP CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In order to solve the above problems, the patent document CN109394571A discloses a composition containing an aqueous nonionic polyurethane dispersion, which can make the hair naturally strong and prolong the duration of the fullness of the hair. However, since the polyurethane is attached to the hair, it is not conducive to Cationic conditioners work attached to the hair and therefore are not ideal for antistatic effects on the hair

Method used

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  • Water-based modified polyurethane dispersion, application thereof and hair conditioner prepared from the same
  • Water-based modified polyurethane dispersion, application thereof and hair conditioner prepared from the same
  • Water-based modified polyurethane dispersion, application thereof and hair conditioner prepared from the same

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0087] Example 1 Preparation of Waterborne Modified Polyurethane Dispersion-1

[0088]

[0089] Among them, m, n, p, q, r, t, u represent the number of repeating units,

[0090] m, n, p, q are independently selected from 0-20, m, n, p, q cannot be 0 at the same time, r is from 25-30, t is from 6, u is from 15-25.

[0091] Add 60g of (S1) IPDI (isophorone diisocyanate), 63.6g (S2) PTMEG2000 (polytetrahydrofuran ether glycol), 40g (S4) YmerTMN120 and 0.0662g (S9) BiCAT8108 catalyst, heat up to 80°C for 1 hour, cool down to 55°C, Add 11.8g (S6) neopentyl glycol and 36g (S7) acetone, raise the temperature to 75°C for reaction, take samples every 1h to measure NCO, until NCO reaches the theoretical value, stop the reaction.

[0092] Cool down to 55°C, add 108g (S7) acetone, cool down to 30°C, pour the prepared prepolymer into a dispersion cup, add 332g (S8) deionized water under high-speed shear conditions of 1500r / min, to obtain Aqueous polyurethane emulsion, then add 0.71...

Embodiment 2

[0094] Example 2 Preparation of Waterborne Modified Polyurethane Dispersion-2

[0095]

[0096] Among them, m, n, p, q, r, t, u represent the number of repeating units,

[0097] m, n, p, q are independently selected from 0-20, m, n, p, q cannot be 0 at the same time, r is from 25-30, t is from 4, u is from 15-25.

[0098] Add 60g of (S1) IPDI (isophorone diisocyanate), 40g (S2) PTMEG2000 (polytetrahydrofuran ether glycol), 40g (S4) YmerTMN120 and 0.0585g (S9) BiCAT 8108 catalyst, heat up to 80°C for 1 hour, cool down to 55°C and add 11.6g (S6) neopentyl glycol and 31.32g (S7) acetone were heated to 75°C for reaction, and NCO was measured every 1 hour until NCO reached the theoretical value, and the reaction was stopped.

[0099]Cool down to 55°C, add 93.98g of acetone, cool down to 30°C, pour the prepared prepolymer into a dispersion cup, add 289g (S8) deionized water under high-speed shear conditions of 1500r / min to obtain water-based polyurethane Emulsion, then add ...

Embodiment 3

[0101] Example 3 Preparation of Waterborne Modified Polyurethane Dispersion-3

[0102]

[0103] Among them, m, n, p, q, r, t, u represent the number of repeating units,

[0104] m, n, p, q are independently selected from 0-20, m, n, p, q cannot be 0 at the same time, r is from 25-30, t is from 1, u is from 15-25.

[0105] Add 60g of (S1) IPDI (isophorone diisocyanate), 50g (S2) PTMEG2000 (polytetrahydrofuran ether glycol), 40g (S4) YmerTMN120 and 0.0615g (S9) BiCAT 8108 catalyst, heat up to 80°C for 1 hour, cool down to 55°C and add 11.6g (S6) neopentyl glycol and 33.5g (S7) acetone were heated up to 75°C for reaction, and NCO was measured every 1 hour until NCO reached the theoretical value, and the reaction was stopped.

[0106] Cool down to 55°C, add 100g (S7) acetone, cool down to 30°C, pour the prepared prepolymer into a dispersion cup, add 307g (S8) deionized water under high-speed shear conditions of 1500r / min, to obtain Aqueous polyurethane emulsion, then add ...

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Abstract

The invention provides a water-based modified polyurethane dispersion. The water-based modified polyurethane dispersion is prepared from the following raw material components through reaction: S1, at least one diisocyanate; S2, macromolecular polyol; S3, polyglutamic acid; S4, at least one monohydric alcohol and / or dihydric alcohol with a main chain and / or a side chain containing a polyoxyethylene chain segment; S5, at least one diamine chain extender containing reactive hydrogen; S6, at least one dihydric alcohol micromolecule chain extender containing reactive hydrogen, namely a catalyst; S7, a low-boiling-point organic solvent; and S8, water. The water-based modified polyurethane dispersion has the advantages of good film-forming elasticity, high glossiness, good toughness, moderate hardness and non-sticky hand feeling, and can be used as a hair conditioner.

Description

technical field [0001] The invention relates to the field of cleaning and care, in particular to a water-based modified polyurethane dispersion and its use and hair conditioner prepared therefrom. Background technique [0002] With the continuous improvement of living standards, people continue to put forward new demands for personal cleaning products. At present, problems such as dry and frizzy hair, prone to static electricity and unmanageable hair are more and more concerned by people. It has become the simplest and most effective way to solve these problems through shampoo. [0003] Commercially available shampoos generally solve the problems of dry and frizzy hair, prone to static electricity and difficult to manage by adding cationic conditioning agents, such as polyquaternium salts or cationic guar gum. However, due to their good water solubility, most of them When shampooing and rinsing the lather, it gets washed away, making it less effective. In addition, some sh...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08G18/75C08G18/66C08G18/48C08G18/32C08G18/60C08J3/03A61K8/87A61Q5/12A61Q5/00
CPCC08G18/755C08G18/6685C08G18/6674C08G18/4808C08G18/4854C08G18/4825C08G18/603C08G18/4054C08J3/03A61K8/87A61Q5/12A61Q5/006
Inventor 李棒棒胡海东赵驰厉涛许诺贾海东孙家宽
Owner WANHUA CHEM GRP CO LTD
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