High-temperature-resistant anti-rutting asphalt mixture
An asphalt mixture, anti-rutting technology, applied in the field of asphalt mixture, to achieve appropriate component distribution ratio, improve water stability, and improve the effect of anti-cracking
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Embodiment 1
[0048]S1: Prepare material;
[0049]S2: Preparation of porous addition:
[0050]2-bromo isobutyl bromide, diethyl ether dissolves, stirred for 10 min, resulting in solution A; glycol, diethyl ether dissolves, stirred for 10 min, then placed in an ice water bath, slowly drop the solution A, stir for 16 h at room temperature, resulting in Agent;
[0051]Take the hair distribution, catalyst, 1,1,4,7,10,10-hexamethylene ethylethyltrine and styrene, mixed stirred for 10 min, frozen, evacuated, heated to material in a nitrogen gas, and then placed It was heated under an oil bath at 110 ° C, toluene and alumina were added, and stirred for 15 min, and ethanol was added, and the precipitate was collected, and the vacuum dried at 60 ° C was added to obtain modified polystyrene;
[0052]Changeive polystyrene, toluene dissolved, then add triethyl aluminum toluene solution, stir for 12h, and add left-transcoxy ester in a nitrogen environment, continue to freeze, vacuum 5min, heat to material dissolution, an...
Embodiment 2
[0064]S1: Prepare material;
[0065]S2: Preparation of porous addition:
[0066]2-bromo isobutyl bromide, diethyl ether dissolves, stirred for 15 min to give a solution A; glycol, diethyl ether dissolves, stirred for 15 min, then placed in an ice water bath, slowly add solution A, stir for 18 h at room temperature, resulting in Agent;
[0067]Take the hair distribution, catalyst, 1,1,4,7,10,10-hexamethylene ethylenedica and styrene, mixed for 15 min, frozen, vacuum, heat to material in a nitrogen environment to material dissolution, and then placed It was heated under an oil bath at 112 ° C, toluene and alumina were added, and stirred for 18 min, then ethanol was added, the precipitate was collected, and the vacuum dried at 60 ° C was added to obtain modified polystyrene;
[0068]Changed polystyrene, toluene dissolved, then add triethyl aluminum toluene solution, stir for 13 h, and adding left-transcoxy ester in a nitrogen environment, continues to freeze, vacuum 6min, heating to material disso...
Embodiment 3
[0080]S1: Prepare material;
[0081]S2: Preparation of porous addition:
[0082]2-bromo isobutyl bromide, diethyl ether dissolves, stirred for 20 min, to obtain solution A; glycol, diethyl ether dissolve, stirred for 20min, then placed in an ice water bath, slowly drop it slowly, stirred at room temperature for 20 h, resulting in Agent;
[0083]Take the hair distribution, catalyst, 1, 1, 4, 7, 10, 10-hexamethylene ethylenedica and styrene, mixed for 20 min, frozen, evacuated, heat to material in a nitrogen environment, and then placed It was heated at 115 ° C for 7.5 h, toluene and alumina were added, and stirred for 20min, then ethanol was added, and the precipitate was collected, dried at 60 ° C to obtain modified polystyrene;
[0084]Take modified polystyrene, toluene dissolve, then add triethyl aluminum toluene solution, stir for 14 h, and add left-transcoxy ester in a nitrogen, continue to freeze, vacuum 7min, heat until the material is dissolved, and then reacted at 95 ° C 7h, anhydrous e...
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