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Clausena lansium volatile oil microcapsule powder and preparation method thereof

A technology of volatile oil and micro-oil, which is applied in the field of flavors and fragrances, to achieve the effect of large-scale industrial continuous production, good repeatability and high yield of microcapsules

Active Publication Date: 2021-03-09
GUANGZHOU HONSEA SUNSHINE BIOTECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It is a common method to prepare microcapsules from volatile oils by spray drying technology. The existing technology evaluates the quality of microcapsules from the indicators of embedding rate, heat resistance, fluidity and sustained release. There is no comprehensive method yet. indicators to evaluate the quality of microcapsules

Method used

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  • Clausena lansium volatile oil microcapsule powder and preparation method thereof
  • Clausena lansium volatile oil microcapsule powder and preparation method thereof
  • Clausena lansium volatile oil microcapsule powder and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0040] Embodiments After weighing the components according to Table 1 and Table 2, the preparation method of the microcapsule powder of the volatile oil of yellow skin described in Example 1 comprises the following steps:

[0041] (1) Prepare the water phase: add water at 70°C to the wall material, stir to dissolve, and stir for 30 minutes to obtain the water phase A with a mass concentration of solids of 50%;

[0042] (2) Prepare the oil phase: mix the emulsifier, antioxidant and volatile oil of wampum bark uniformly at 60°C to obtain the oil phase B;

[0043] (3) Emulsification: Add the oil phase B obtained in the step (2) to the water phase A obtained in the step (1), and stir at a rate of 30000 rpm and a stirring time of 40 min to obtain a coarse emulsion;

[0044] (4) Homogenization, spray drying: the coarse emulsion obtained in step (3) is homogenized, the pressure of homogenization is 30MPa, and the number of times of homogenization is 3 times, and the homogeneous liqui...

Embodiment 2

[0046] EXAMPLES After weighing the components according to Table 1 and Table 2, the preparation method of the microcapsule powder of yellow skin volatile oil described in Example 2 comprises the following steps:

[0047](1) Prepare the water phase: add water at 60°C to the wall material, stir to dissolve, and stir for 30 minutes to obtain the water phase A with a mass concentration of solids of 40%;

[0048] (2) Prepare the oil phase: mix the emulsifier, antioxidant and volatile oil of yellow bark uniformly at 40°C to obtain the oil phase B;

[0049] (3) Emulsification: Add the oil phase B obtained in step (2) to the water phase A obtained in step (1), and stir at a rate of 10000 rpm for 20 minutes to obtain a coarse emulsion;

[0050] (4) Homogenization, spray drying: the coarse emulsion obtained in step (3) is homogenized, the pressure of homogenization is 20MPa, and the number of times of homogenization is 2 times, the homogeneous liquid is incubated, and the temperature of...

Embodiment 3

[0052] Embodiment After weighing the components according to Table 1 and Table 2, the preparation method of the microcapsule powder of the volatile oil of yellow skin described in Example 3 comprises the following steps:

[0053] (1) Prepare the water phase: add water at 65°C to the wall material, stir to dissolve, and stir for 30 minutes to obtain the water phase A with a solid content of 45%;

[0054] (2) Prepare the oil phase: mix the emulsifier, antioxidant and volatile oil of wampum bark uniformly at 50°C to obtain the oil phase B;

[0055] (3) Emulsification: Add the oil phase B obtained in step (2) to the water phase A obtained in step (1), and stir at a rate of 10000 rpm for 20 minutes to obtain a coarse emulsion;

[0056] (4) Homogenization, spray drying: the coarse emulsion obtained in step (3) is homogenized, the pressure of homogenization is 25MPa, and the number of times of homogenization is 2 times, the homogeneous liquid is incubated, and the temperature of insu...

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Abstract

The invention discloses clausena lansium volatile oil microcapsule powder, and relates to the field of flavors and fragrances. The clausena lansium volatile oil microcapsule powder comprises the following components in parts by weight: 30-50 parts of clausena lansium volatile oil, 50-70 parts of a wall material, 0.5-3 parts of an emulsifier and 0.05-0.5 part of an antioxidant. The clausena lansiumvolatile oil microcapsule powder provided by the invention has a glass transition temperature of 80 DEG C or above, and has good heat resistance, embedding rate and storage resistance.

Description

technical field [0001] The invention relates to the field of flavors and fragrances, in particular to a microcapsule powder of volatile oil of yellow skin and a preparation method thereof. Background technique [0002] Yellow skin is a characteristic fruit in southern China. It is rich in vitamin C, sugar, organic acids and pectin. Both the peel and the core can be used as medicine. The yellow skin is deeply loved by consumers because of the special aroma of the fruit and peel. This special aroma is mainly composed of volatile oil components. It is a common method to prepare microcapsules from volatile oils by spray drying technology. The existing technologies all evaluate the quality of microcapsules from the indicators of embedding rate, heat resistance, fluidity, and sustained release. There is no comprehensive method yet. indicators to evaluate the quality of microcapsules. [0003] Glass transition temperature T g It is an important indicator of spray drying to form ...

Claims

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Application Information

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IPC IPC(8): A23L27/12A23L27/00C11B9/02
CPCA23L27/12A23L27/72C11B9/025A23V2002/00A23V2250/18A23V2200/222A23V2200/02A23V2300/14A23V2250/21A23V2250/5028A23V2250/5114A23V2250/2132A23V2250/214A23V2250/72A23V2250/2134A23V2250/5118A23V2250/5112A23V2250/5432A23V2250/6416A23V2250/616A23V2250/28A23V2250/5072A23V2250/5488A23V2250/6402A23V2250/5036A23V2250/5086A23V2250/5044A23V2250/628A23V2250/5026A23V2250/54252A23V2250/511A23V2300/10Y02P20/54
Inventor 夏源明罗安东陈志强李云云庄晓慈
Owner GUANGZHOU HONSEA SUNSHINE BIOTECH CO LTD
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