Platinum quantum dot doped graphene-based electric heating plate and electric heating device
A graphene-based, electric heating plate technology, applied in the field of nano-materials, can solve the problems of difficulty in controlling the thickness of the graphene heating layer, poor stability of the electric heating plate, and brittle conductive film, etc., to achieve easy product quality, complete functions, The effect of controlling product quality
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Embodiment 1
[0067] Preparation of graphene oxide acetone dispersion: 500 mg of graphite powder was provided, and graphene oxide (Graphene Oxide, GO) was prepared by a modified Hummers method. In order to further obtain few-layer graphene oxide, place graphene oxide in an ice-water bath, use an ultrasonic disperser to sonicate for 10 minutes at a power of 250W, repeat once, take the supernatant, centrifuge, and resuspend in acetone to obtain a thickness ranging from 12 to Graphene oxide acetone dispersion liquid with 20 layers and lateral dimension of 700-1000nm. Concentrate by centrifugation as required to adjust the concentration of the graphene oxide acetone dispersion to 150 mg / ml.
[0068] Preparation of platinum quantum dot-doped graphene dispersion: take 50ml of the graphene oxide acetone dispersion prepared above and add 0.05g of phosphomolybdic acid to it, stir at 600rpm for 10h, centrifuge at 15000rpm for 30min, and collect the first precipitate at the bottom of the centrifuge tu...
Embodiment 2
[0074] Preparation of graphene oxide acetone dispersion: 500 mg of graphite powder was provided, and graphene oxide (Graphene Oxide, GO) was prepared by a modified Hummers method. The prepared graphene oxide was further transferred to a high-temperature carbonization furnace for high-temperature carbonization for 30 s. The high-temperature carbonization furnace was filled with nitrogen gas, and the temperature of the high-temperature carbonization furnace was 1200° C. In order to further obtain few-layer graphene oxide, place the graphene oxide expanded at high temperature in an ice-water bath, use an ultrasonic disperser to sonicate for 20 minutes at a power of 250W, repeat once, take the supernatant, centrifuge, and resuspend in acetone. A graphene oxide acetone dispersion liquid with a thickness ranging from 8 to 15 layers and a lateral dimension of 700 to 1000 nm. Concentrate by centrifugation as required to adjust the concentration of the graphene oxide acetone dispersion...
Embodiment 3
[0081] Preparation of graphene oxide acetone dispersion: 500 mg of graphite powder was provided, and graphene oxide (Graphene Oxide, GO) was prepared by a modified Hummers method. The prepared graphene oxide was further transferred to a high-temperature carbonization furnace for high-temperature carbonization for 60 seconds. The high-temperature carbonization furnace was filled with argon gas, and the temperature of the high-temperature carbonization furnace was 1000° C. In order to further obtain few-layer graphene oxide, place the graphene oxide expanded at high temperature in an ice-water bath, use an ultrasonic disperser to sonicate for 30 minutes at a power of 250W, repeat once, take the supernatant, centrifuge, and resuspend in acetone to obtain Graphene oxide acetone dispersion with a thickness ranging from 1 to 8 layers and a lateral dimension of 700 to 1000 nm. Concentrate by centrifugation as required to adjust the concentration of the graphene oxide acetone dispersi...
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