An environment-friendly high temperature and salt resistant calcium modified natural polymer fluid loss reducer
A technology of natural polymer and fluid loss reducer, which is applied in the direction of chemical instruments and methods, drilling compositions, etc. It can solve the problems of low temperature resistance, reduced mud cake bound water content, poor salt and calcium resistance, etc. , to achieve the effect of reducing fluid loss, good compatibility, and strong wall-building effect
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Embodiment 1
[0024] An environment-friendly, high-temperature-resistant, salt-resistant, calcium-modified natural polymer fluid loss reducer mentioned in the present invention is composed of: 25% of pregelatinized starch, 5% of partially hydrolyzed polyacrylamide, 4% of aluminum citrate, ultrafine Calcium carbonate 15%, the balance is deionized water; wherein,
[0025] The partially hydrolyzed polyacrylamide is a commercially available tackifier for polyacrylamide drilling fluid, the relative molecular mass is 3 million, and the degree of hydrolysis is within the range of 20%; the aluminum citrate is a commercially available crosslinking agent product; The superfine calcium carbonate is a commercially available oil and gas reservoir protective agent for drilling fluids, with a particle size range of 400 meshes.
[0026] The preparation method of the present invention comprises the following steps:
[0027] (1) First, dissolve the partially hydrolyzed polyacrylamide in a kneader with an ap...
Embodiment 2
[0036] The environment-friendly, high-temperature, salt-resistant, calcium-modified natural polymer fluid loss reducer mentioned in the present invention is composed of: 20% of carboxymethyl starch, 7% of partially hydrolyzed polyacrylamide, 6% of aluminum citrate, ultrafine Calcium carbonate 20%, the balance is distilled water;
[0037] The partially hydrolyzed polyacrylamide is a commercially available tackifier for polyacrylamide drilling fluid, the relative molecular mass is 5 million, and the degree of hydrolysis is within the range of 40%; the aluminum citrate is a commercially available crosslinking agent product; The superfine calcium carbonate is a commercially available oil and gas layer protective agent for drilling fluids, and the particle size range is in the range of 1200 meshes.
[0038] According to the production steps of Example 1, product 2 was prepared.
Embodiment 3
[0040] An environment-friendly, high-temperature, salt-resistant, calcium-modified natural polymer fluid loss reducer mentioned in the present invention is composed of: cationic starch starch 30%, partially hydrolyzed polyacrylamide 5%, aluminum citrate 3%, ultrafine carbonic acid Calcium 10%, the balance is drinking tap water;
[0041] The partially hydrolyzed polyacrylamide is a commercially available flocculant for polyacrylamide drilling fluid, the relative molecular mass is 4 million, and the degree of hydrolysis is within the range of 30%; the aluminum citrate is a commercially available crosslinking agent product; the Ultrafine calcium carbonate is a commercially available oil and gas reservoir protective agent for drilling fluids, with a particle size range of 800 mesh.
[0042] According to the preparation steps of Example 1, product three was prepared.
[0043] According to the API experimental procedure, 2% of the three examples of products were added to the satura...
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