A kind of anti-pet agent and its preparation method and application
A pet and intercalation agent technology, applied in the direction of botany equipment and methods, applications, pest repellents, etc., can solve the problems of capsaicin content loss, affecting product batch stability, and poor heat-resistant stability of capsaicin
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Embodiment 1
[0060] A kind of anti-pet agent is prepared by the following method:
[0061] Step 1: Disperse magadiite in deionized water, stir for 3 hours, and sonicate for 30 minutes to obtain a suspension of magadiite. The mass ratio of magadiite to deionized water is 1:50; Wherein the magadiite has an average particle size of 30nm.
[0062] The second step: add the aliphatic amino-terminated hyperbranched polyamide into the acetic acid solution with a volume fraction of 1%, adjust the pH value to 5.0 with 1mol / L NaOH solution after fully dissolving, and then slowly add the mixed solution to the first In the magadisite suspension obtained in step 1, heat to 80°C, stir and react for 6h, centrifuge the mixture at 5000r / min for 10min, then filter it with a 0.45μm microporous membrane, and wash it with distilled water until neutral to obtain Intercalation modified magadiite, the mass ratio of aliphatic amino-terminated hyperbranched polyamide to acetic acid solution is 1:100; the molecular ...
Embodiment 2
[0066] The first step: disperse the montmorillonite in deionized water, stir for 3 hours, and ultrasonicate for 30 minutes to obtain a montmorillonite suspension. The mass ratio of the montmorillonite to deionized water is 1:50; the average particle size of the montmorillonite is The diameter is 30nm.
[0067] The second step: add the aliphatic amino-terminated hyperbranched polyamide into the acetic acid solution with a volume fraction of 1%, adjust the pH value to 5.0 with 1mol / L NaOH solution after fully dissolving, and then slowly add the mixed solution to the first The montmorillonite suspension obtained in step 1 was heated to 80°C, stirred for 6 hours, the mixture was centrifuged at 5000r / min for 10 minutes, then filtered through a 0.45μm microporous membrane, and washed with distilled water until neutral to obtain intercalation Modified montmorillonite, the mass ratio of aliphatic amino-terminated hyperbranched polyamide to acetic acid solution is 1:100; the molecular ...
Embodiment 3
[0070] The only difference from Example 1 is that the inorganic carrier in this example is sepiolite modified with aliphatic amino-terminated hyperbranched polyamide.
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