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Method for testing permanganate index

A technology of permanganate index and testing method, applied in testing field

Active Publication Date: 2020-04-17
HANGZHOU GREAN WATER SCI & TECH INC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Existing technology The on-line monitoring of permanganate index and laboratory automation instruments have developed rapidly in China in recent years, but the instruments of various manufacturers will have large errors when measuring water samples and environmental standard samples

Method used

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  • Method for testing permanganate index
  • Method for testing permanganate index
  • Method for testing permanganate index

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0120] 1. Adopt the online permanganate index analyzer produced by Hangzhou Lvjie Environmental Technology Co., Ltd.;

[0121] 2. The adjustment of the digestion module is adopted.

[0122] Heat the aluminum block at a constant temperature of 110°C, and read the temperature from normal temperature to temperature and close to boiling; take the difference between the temperature of the aluminum block and the temperature of the reaction cup per second as the ordinate, and the derivative of the reaction pool temperature at the corresponding time as the abscissa , to perform straight line fitting to obtain the slope K1. Using the GB11892 method, the temperature of the boiling water is determined to be 100°C, the difference between the temperature of the boiling water and the Erlenmeyer flask per second is the ordinate, and the derivative of the reaction solution temperature in the Erlenmeyer flask at the corresponding time is the abscissa, and a straight line is fitted to obtain th...

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PUM

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Abstract

The invention provides a method for testing permanganate index, which comprises the following steps: (a) a sample to be tested, a sulfuric acid solution and a potassium permanganate solution are mixed, the mixture is heated to a temperature of 94.6-94.9 DEG C according to t<ideal>= 94.831-77.737*exp(-t / 113.082), and an oxidation reaction is performed during the heating process, wherein the volumeratio of the to-be-tested sample to the sulfuric acid solution to the potassium permanganate solution is 20: 1: 2, the concentration of the potassium permanganate solution is 0.31-0.33 g / L, the concentration of the sulfuric acid solution is 485-495 g / L, and the concentration of a sodium oxalate solution is 0.83-0.85 g / L; (b) excessive sodium oxalate solution is added for reduction reaction, potassium permanganate solution is dropwise added until the potential value changes suddenly, and the titration time is recorded, wherein the titration rate is 25mL / 1000s; and (c) the permanganate index iscalculated according to the titration time and a formula. The permanganate index measured by adopting the method is relatively high in accuracy.

Description

technical field [0001] The invention belongs to the technical field of testing, in particular to a method for testing permanganate index. Background technique [0002] The permanganate index is one of the basic parameters for evaluating the quality of surface water, which characterizes the degree of organic pollution in the water. [0003] Existing technology The on-line monitoring of permanganate index and laboratory automation instruments have developed rapidly in China in recent years, but the instruments of various manufacturers will have large errors when measuring water samples and environmental standard samples. Therefore, it is particularly important to develop a test method for permanganate index with higher accuracy. Contents of the invention [0004] In view of this, the object of the present invention is to provide a method for testing the permanganate index, which has higher accuracy. [0005] The invention provides a kind of test method of permanganate inde...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N31/16
CPCG01N31/16Y02A20/20
Inventor 汤杰龙见翔崔海松张立鹏于圣文黄升
Owner HANGZHOU GREAN WATER SCI & TECH INC
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