A kind of carbon self-coated micron tungsten oxide, negative electrode material, battery and preparation method
A carbon self-coating and tungsten oxide technology, which is applied in the preparation/purification of carbon, tungsten oxide/tungsten hydroxide, battery electrodes, etc., can solve the problems of low specific capacity and poor cycle stability of electrode materials, and achieve good cycle performance , stable charging and discharging, and high rate performance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0041] figure 1 A schematic flowchart of a preparation method of carbon self-coated micron-scale tungsten oxide provided in the embodiments of the present application, such as figure 1 As shown, the method mainly includes the following steps.
[0042] Step S100 : a precursor of carbon self-coated micron-sized tungsten oxide is prepared by a self-polymerization reaction stirred in a water bath.
[0043] In an optional embodiment, the reaction to prepare the precursor of carbon self-coated micron-sized tungsten oxide includes:
[0044] Step S101 : adding a carbon source and a tungsten source into a dispersant, dispersing and mixing, to obtain a mixed solution.
[0045] In an optional embodiment, the carbon source is a mixture of two or more of dopamine hydrochloride, polyvinylpyrrolidone and urotropine; the tungsten source is sodium tungstate, lithium tungstate and tungsten One or more mixtures of ammonium acid; the dispersing agent is one or two mixtures of absolute ethanol ...
Embodiment 1
[0067] At room temperature, 0.4g of tungstic acid, 1g of polyvinylpyrrolidone and 0.1g of PDA were added to the mixed solution of 100mL of water and 150mL of ethanol to disperse and mix, and after stirring for 5, 80mL of the above solution was taken in a 100mL beaker to carry out self-polymerization with water bath stirring. The reaction was carried out at a reaction temperature of 50° C. and a holding time of 5 hours. After the reaction was completed, the product was subjected to centrifugal drying treatment, and then vacuum dried at 60° C. for 12 hours. After that, the dried samples were placed in a porcelain boat at 500 °C, and the heating rate was 2 °C min. -1 , the holding time is 2h, and the sintering atmosphere is argon.
Embodiment 2
[0069] At room temperature, 0.5g of tungstic acid, 1g of polyvinylpyrrolidone and 0.1g of PDA were added to the mixed solution of 100mL of water and 150mL of ethanol to disperse and mix, and after stirring for 5 years, 80mL of the above solution was taken in a 100mL beaker to carry out self-water bath stirring. In the polymerization reaction, the reaction temperature is 80°C, and the holding time is 5h. After the reaction is completed, the product is subjected to centrifugal drying treatment, and then vacuum dried at 60°C for 12h. After that, the dried samples were placed in a porcelain boat at 500 °C, and the heating rate was 2 °C min. -1 , the holding time is 2h, and the sintering atmosphere is argon.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com