Glucosamine bone glue peptide calcium granules
A technology of granules and collagen peptides, which is applied in the field of medicine, can solve problems such as hard-to-reach and increase bone density, and achieve the effect of improving resistance, increasing bone density, and synergistic bone function
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Embodiment 1
[0028] In parts by weight, take 45 parts of bone collagen peptide, 25 parts of glucosamine sulfate calcium salt, 13 parts of Antarctic krill oil, 7 parts of isomaltooligosaccharide, 4 parts of D-ribose, 4 parts of oat essence, 5 parts of Seaweed polysaccharide, 10 parts of shrimp powder, 7 parts of vitamin D3, 7 parts of fish oil, and appropriate amount of microcrystalline cellulose, magnesium stearate, and silicon dioxide were used to prepare glucosamine bone gel peptide calcium granules.
[0029]Wherein the preparation method of glucosamine sulfate calcium salt is as follows: get 1kg chitin and 1L 1-butyl-3-methylimidazole methyl sulfate, 3L mass concentration is 25% sulfuric acid and mix under the condition of 40 ℃ Stir to obtain a crude mother liquor, then use a diaphragm pump to continuously pump it into a microporous membrane filter to filter to obtain a fine mother liquor; mix the prepared fine mother liquor with 1-propylsulfanoyl-3-methylimidazolium bisulfate ionic liqu...
Embodiment 2
[0031] In parts by weight, take 40 parts of bone collagen peptide, 20 parts of glucosamine sulfate calcium salt, 10 parts of N-acetylglucosamine, 10 parts of Antarctic krill oil, 5 parts of isomaltooligosaccharide, 3 parts of D-ribose , 2 parts of oat essence, 3 parts of seaweed polysaccharide, 8 parts of shrimp powder, 5 parts of vitamin D3, 5 parts of fish oil, and appropriate amount of microcrystalline cellulose, magnesium stearate, and silicon dioxide to prepare glucosamine bone glue peptide calcium granules.
[0032] Wherein the preparation method of glucosamine sulfate calcium salt is as follows: get 1kg chitin and 2L 1-butyl-3-methylimidazole methyl sulfate, 4L mass concentration is 20% sulfuric acid and mix and stir under the condition of 35 ℃ Obtain thick mother liquor, then use diaphragm pump to continuously pump into microporous membrane filter and filter to obtain fine mother liquor; The degradation solution was prepared by mixing and incubating at 80°C for 3 hours...
Embodiment 3
[0034] In parts by weight, take 50 parts of bone collagen peptide, 30 parts of glucosamine sulfate calcium salt, 15 parts of Antarctic krill oil, 10 parts of isomaltooligosaccharide, 6 parts of D-ribose, 5 parts of oat essence, 7 parts of Seaweed polysaccharide, 13 parts of shrimp skin powder, 9 parts of vitamin D3, 9 parts of fish oil, and appropriate amount of microcrystalline cellulose, magnesium stearate, and silicon dioxide were used to prepare glucosamine bone gel peptide calcium granules.
[0035] Wherein the preparation method of glucosamine sulfate calcium salt is as follows: get 1kg chitin and 1L 1-butyl-3-methylimidazole methyl sulfate, 2L mass concentration is 30% sulfuric acid and mix under the condition of 45 ℃ Stir to obtain a crude mother liquor, then use a diaphragm pump to continuously pump it into a microporous membrane filter to filter to obtain a fine mother liquor; mix the prepared fine mother liquor with 1-propylsulfanoyl-3-methylimidazolium bisulfate ion...
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