UV-CTP photosensitive adhesive and preparation and testing method thereof
A UV-CTP, photosensitive adhesive technology, applied in the photosensitive adhesive field, can solve the problems of insufficient alkali resistance and solvent resistance, damage to the photosensitive film layer, etc., and achieve excellent alcohol resistance, high printing resistance, and wide developing latitude. Effect
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[0065] The second aspect of the present invention provides a preparation method of UV-CTP photosensitive glue, which includes the following steps: adding the above components into the solvent in sequence according to the formula, stirring for 10-20 hours, and filtering after complete dissolution to obtain the photosensitive glue.
[0066] In the present invention, the solvent can be selected from one of methyl ethyl ketone, butyrolactone, ethylene glycol ethyl ether, ethylene glycol monoethyl ether, ethylene glycol monomethyl ether, butyl acetate, dioxane, tetrahydrofuran, butanone one or more combinations.
[0067] Preferably, the solvent is a mixed solvent of butyrolactone, ethylene glycol ether, butanone, and dioxane.
[0068] As more preferably, the volume ratio of butyrolactone, ethylene glycol ethyl ether and butanone in the mixed solvent is (0-10%):(20%-90%):(0-60%).
[0069] As most preferably, the volume ratio of butyrolactone, ethylene glycol ethyl ether and butanon...
Embodiment 1
[0093] Embodiment 1 provides a kind of UV-CTP photosensitive adhesive, by mass fraction, at least includes the following components, coloring dye 2%, photosensitizer 20%, film-forming resin 45%, alcohol-resistant resin 25%, solvent resistance 3% , Monofunctional anhydride 5%.
[0094] The colored dye is crystal violet; the sensitizer is 2,1,4-diazonaphthoquinone sulfonate, purchased from Shanghai Dajin Photosensitive Material Co., Ltd., the model is NAC-4; the film-forming resin is plastic Phenolic resin, purchased from Benxi Ruishida Chemical Co., Ltd., model is BX-30; the capacitance resistance agent is triphenyl phosphate; the monofunctional anhydride is tetrahydrophthalic anhydride.
[0095] The alcohol-resistant resin, in parts by mass, includes the following components: 30 parts of (meth)acrylate, 25 parts of acrylonitrile, 10 parts of styrene, 50 parts of acrylamide, N-[4-(sulfonamide)benzene base] 80 parts of acrylamide; the preparation method of the alcohol-resistant...
Embodiment 2
[0101] Embodiment 2 provides a kind of UV-CTP photosensitive adhesive, in terms of mass fraction, at least includes the following components, coloring dye 0.5%, photosensitizer 30%, film-forming resin 50%, alcohol-resistant resin 16%, solvent resistance 1.5% , Monofunctional anhydride 2%.
[0102] The preparation method and testing method of the UV-CTP photosensitive glue are the same as in Example 1.
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