Graphene doped Cu/Cu2O nano photocatalytic coating and preparation method thereof
A catalytic coating, graphene technology, applied in metal/metal oxide/metal hydroxide catalysts, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the problem that photolysis research is rarely reported, etc. The effect of strong visible light response, enhanced light absorption, good degradation effect
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[0022] A graphene-doped Cu / Cu 2 The preparation method of O nano photocatalytic coating, comprises the following steps:
[0023] 1) Pre-treat the workpiece to clean off the dust, grease and rust on the surface of the workpiece;
[0024] 2) Preparation of graphene-doped Cu / Cu 2 O composite slurry: (1) take Cu 2 O powder is dispersed in alcohol aqueous solution, and ultrasonic treatment is carried out under the condition of magnetic stirring; (2) after the ultrasonic is finished, add adhesive solution and Cu powder, continue to stir evenly; (3) dropwise add graphene oxide powder, the solution continues Magnetically stirred evenly to obtain graphene-doped Cu / Cu 2 O composite slurry;
[0025] Among them, Cu 2 The mass ratio of O powder, Cu powder, graphene oxide powder is 75:20:5, and binder solution is the polyvinyl alcohol aqueous solution or the epoxy polyester powder coating that mass percent is 3-5%;
[0026] 3) The above-mentioned slurry is pressed on the surface of th...
Embodiment 1
[0030] A graphene-doped Cu / Cu 2 The preparation method of O nano photocatalytic coating, comprises the following steps:
[0031] 1) Pre-treat the workpiece to clean off the dust, grease and rust on the surface of the workpiece;
[0032] 2) Preparation of graphene-doped Cu / Cu 2 O composite slurry: (1) take Cu 2 O powder is dispersed in alcohol aqueous solution, and ultrasonic treatment is carried out under the condition of magnetic stirring; (2) after the ultrasonic is finished, add adhesive solution and Cu powder, continue to stir evenly; (3) dropwise add graphene oxide powder, the solution continues Magnetically stirred evenly to obtain graphene-doped Cu / Cu 2 O composite slurry;
[0033] Among them, Cu 2 The mass ratio of O powder, Cu powder, graphene oxide powder is 75:20:5, and binder solution is the polyvinyl alcohol aqueous solution that mass percentage is 3%;
[0034] 3) The above-mentioned slurry is pressed on the surface of the pretreated workpiece by a mechanica...
Embodiment 2
[0038] A graphene-doped Cu / Cu 2 The preparation method of O nano photocatalytic coating, comprises the following steps:
[0039] 1) Pre-treat the workpiece to clean off the dust, grease and rust on the surface of the workpiece;
[0040] 2) Preparation of graphene-doped Cu / Cu 2 O composite slurry: (1) take Cu 2 O powder is dispersed in alcohol aqueous solution, and ultrasonic treatment is carried out under the condition of magnetic stirring; (2) after the ultrasonic is finished, add adhesive solution and Cu powder, continue to stir evenly; (3) dropwise add graphene oxide powder, the solution continues Magnetically stirred evenly to obtain graphene-doped Cu / Cu 2 O composite slurry;
[0041] Among them, Cu 2 The mass ratio of O powder, Cu powder, graphene oxide powder is 75:20:5, and binder solution is the polyvinyl alcohol aqueous solution that mass percentage is 5%;
[0042] 3) The above-mentioned slurry is pressed on the surface of the pretreated workpiece by a mechanica...
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