Method for enhancing magnetism of bismuth ferrite nano powder based on size effect
A nano-powder and size-effect technology, which is applied in nanotechnology, nanotechnology, nanotechnology, etc. for materials and surface science, can solve the problems of weak ferromagnetism and easy generation of impurities in bismuth ferrite, and achieve enhanced ferromagnetic properties , magnetic enhancement, high purity effect
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[0029] Embodiment 1: A kind of method for strengthening the magnetism of bismuth ferrite nanopowder based on the size effect in the present embodiment is carried out according to the following steps:
[0030] Step 1, add 125mL ethylene glycol monomethyl ether (CH 3 OCH 2 CH 2 0.05mol bismuth nitrate pentahydrate (Bi(NO 3 ) 3 ·5H 2 O) and 0.05mol of iron nitrate nonahydrate (Fe(NO 3 ) 3 9H 2 0), after finishing, dropwise adding 125 μ L concentration is the dilute nitric acid of 0.1mol / L, makes the pH value of solution in the scope of 3~4;
[0031] Step 2, continue to stir, add the monohydrate citric acid (C 6 h 8 o 7 ·H 2 (2), stir well, and citric acid is used as complexing agent, makes metal ion form complex compound, then adds 62.5mL ethylene glycol (dispersant), stirs;
[0032] Step 3, then place it in a water bath at 60°C for 1 hour with magnetic stirring at a stirring speed of 550r / min, and then place it in a blast drying oven at 100°C for 10 hours to obtain a...
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