Preparation method for high-strength water-resistant rock-soil repairing material used for ancient buildings
A repairing material and technology for ancient buildings, which is applied in the field of preparation of high-strength water-resistant rock and soil ancient building repairing materials, can solve problems such as poor water resistance, and achieve the effects of improving mechanical properties, good gloss and color retention, and good storage stability
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Embodiment 1
[0031] In parts by weight, weigh 10 parts of carboxymethyl styrene-butadiene latex, 20 parts of natural hydraulic lime, 5 parts of methyl methacrylate, 10 parts of acrylic acid, 1 part of butyl acrylate, 1 part of ammonium persulfate, 40 parts of Mix carboxymethyl styrene-butadiene latex with deionized water, stir for 10 minutes at a temperature of 60°C and a stirring speed of 200r / min to obtain reaction solution A, add natural hydraulic lime to the reaction solution, Continue to stir for 5 minutes to obtain the reaction solution B. Add ammonium persulfate to the reaction solution B. After stirring for 5 minutes at a stirring speed of 400 r / min, add methyl methacrylate, acrylic acid and butyl acrylate, and continue stirring for 6 hours. Obtain base body liquid, be that the pH value of 25% ammonia water adjustment base body liquid is 7 with mass fraction, obtain modified natural hydraulic lime; Mix dicumyl peroxide, maleic anhydride and acetone by mass ratio 1: 10: 20 Mix evenl...
Embodiment 2
[0033] In parts by weight, weigh 12 parts of carboxymethyl styrene-butadiene latex, 30 parts of natural hydraulic lime, 8 parts of methyl methacrylate, 12 parts of acrylic acid, 5 parts of butyl acrylate, 2 parts of ammonium persulfate, 45 parts Mix the carboxymethyl styrene-butadiene latex and deionized water, and stir for 15 minutes at a temperature of 65° C. and a stirring speed of 250 r / min to obtain the reaction solution A. Add natural hydraulic lime to the reaction solution, Continue to stir for 8 minutes to obtain the reaction solution B. Add ammonium persulfate to the reaction solution B. After stirring for 8 minutes at a stirring speed of 450 r / min, add methyl methacrylate, acrylic acid and butyl acrylate, and continue stirring for 7 hours. Obtain base body liquid, be that the pH value of 25% ammonia water adjustment base body liquid is 7 with mass fraction, obtain modified natural hydraulic lime; Mix dicumyl peroxide, maleic anhydride and acetone by mass ratio 1: 10: ...
Embodiment 3
[0035] In parts by weight, 15 parts of carboxymethyl styrene-butadiene latex, 40 parts of natural hydraulic lime, 10 parts of methyl methacrylate, 15 parts of acrylic acid, 10 parts of butyl acrylate, 3 parts of ammonium persulfate, 50 parts Mix carboxymethyl styrene-butadiene latex and deionized water with a temperature of 70°C and a stirring speed of 300r / min for 20min to obtain reaction solution A. Add natural hydraulic lime to the reaction solution, Continue to stir for 10 minutes to obtain the reaction solution B. Add ammonium persulfate to the reaction solution B. After stirring for 10 minutes at a stirring speed of 500 r / min, add methyl methacrylate, acrylic acid and butyl acrylate, and continue stirring for 8 hours. Obtain base body liquid, be that the pH value of 25% ammonia water adjustment base body liquid is 8 with mass fraction, promptly obtain modified natural hydraulic lime; Mix dicumyl peroxide, maleic anhydride and acetone by mass ratio 1: 10: 20 Mix evenly to...
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