Flame-retardant epoxy resin
An epoxy resin, flame retardant technology, applied in the field of flame retardant epoxy resin, can solve the problems of poor thermal performance of epoxy resin, poor flame retardancy, human injury, etc., achieve low volatility, good electrical insulation, The effect of improving flame retardancy
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Embodiment 1
[0034] a. Reserve raw materials, the epoxy resin raw materials include by weight: 10-20 parts of cyclic hydrocarbon compounds, 10-15 parts of flame retardant and curing compounds, 60-65 parts of epoxy resin monomers, flame retardant micro Capsule 10-15 parts, modified phenolic resin 8-10 parts, expanded graphite 0.5-1 part, curing agent 3-5 parts, talcum powder 1.5-4.5 parts, quartz sand 2-5 parts, defoamer 0.5-1 part , 0.2-1.5 copies of leveling agent;
[0035] b, with 60-65 parts by weight of epoxy resin monomer, 10-15 parts by weight of flame-retardant microcapsules, 0.5-1 parts by weight of expanded graphite and 8-10 parts by weight of modified phenolic resin, mechanically After stirring for 45-60min, then 30-70kHz ultrasonic dispersion for 30-45min;
[0036] c. After ultrasonically dispersing the mixed system obtained in step b to remove the dispersion medium, add 10-15 parts of flame retardant and curing compound; raise the temperature of the added flame retardant and c...
Embodiment 2
[0041] No flame retardant microcapsules added:
[0042] a. Reserve raw materials, the epoxy resin raw materials include by weight: 10-20 parts of cyclic hydrocarbon compound, 10-15 parts of flame retardant and curing compound, 60-65 parts of epoxy resin monomer, modified phenolic resin 8-10 parts, 0.5-1 part of expanded graphite, 3-5 parts of curing agent, 1.5-4.5 parts of talcum powder, 2-5 parts of quartz sand, 0.5-1 part of defoamer, 0.2-1.5 parts of leveling agent;
[0043] b. 60-65 parts by weight of epoxy resin monomer, 0.5-1 parts by weight of expanded graphite and 8-10 parts by weight of modified phenolic resin are mechanically stirred at 400-600rpm for 45-60min, and then stirred at 30-70 kilohertz Ultrasonic dispersion for 30-45min;
[0044]c. After ultrasonically dispersing the mixed system obtained in step b to remove the dispersion medium, add 10-15 parts of flame retardant and curing compound; raise the temperature of the added flame retardant and curing compound...
Embodiment 3
[0049] No flame retardant microcapsules and expanded graphite:
[0050] a. Reserve raw materials, the epoxy resin raw materials include by weight: 10-20 parts of cyclic hydrocarbon compound, 10-15 parts of flame retardant and curing compound, 60-65 parts of epoxy resin monomer, modified phenolic resin 8-10 parts, 3-5 parts of curing agent, 1.5-4.5 parts of talcum powder, 2-5 parts of quartz sand, 0.5-1 part of defoamer, 0.2-1.5 parts of leveling agent;
[0051] b. 60-65 parts by weight of epoxy resin monomer and 8-10 parts by weight of modified phenolic resin are mechanically stirred at 400-600 rpm for 45-60 minutes, and then ultrasonically dispersed at 30-70 kilohertz for 30-45 minutes;
[0052] c. After ultrasonically dispersing the mixed system obtained in step b to remove the dispersion medium, add 10-15 parts of flame retardant and curing compound; raise the temperature of the added flame retardant and curing compound to 100-120 ° C, and use 300- 500rpm for mechanical st...
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