Preparation method of graphene oxide/attapulgite/polyvinyl alcohol ceramic matrix composite membrane
A technology of ceramic matrix and attapulgite, applied in chemical instruments and methods, permeation/dialysis water/sewage treatment, membrane technology, etc., can solve problems such as hindering the dispersion of GO nanosheets, achieve improved membrane flux, and simple preparation process , low-cost effect
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Embodiment 1
[0022] Dissolve 10 g of 3-aminopropyl-triethoxysilane in 1 L of absolute ethanol to form a mixed solution of 10 g / L, and soak the Al2O3 ceramic substrate with a pore size of 0.5 μm in the mixed solution for 5 h , rinsed with deionized water after being taken out, and dried in an oven at 120 °C for 3 h.
[0023] A small amount of PVA was dissolved in water under the condition of heating and stirring at 80 °C to prepare a 1 wt% mass concentration solution for later use.
[0024] Measure 1 ml of 1 mg / L graphene oxide dispersion, 5 mg of attapulgite and 60 mg of 1 wt% PVA solution at a ratio of m(GO:ATP)=1:5, mix and dilute to 15 mL, and the solution was stirred for 30 min, at which point the total mass of the membrane was 6.6 mg.
[0025] Slowly pour the solution into a suction filter bottle, vacuum filter it on the Al2O3 ceramic substrate, completely drain it to form a film, take it out, put it in an oven for 2 h at 50 °C, and prepare GO / ATP / PVA (10%) Composite film such as f...
Embodiment 2
[0027] Dissolve 10 g of 3-aminopropyl-triethoxysilane in 1 L of absolute ethanol to form a mixed solution of 10 g / L, and soak the Al2O3 ceramic substrate with a pore size of 0.2 μm in the mixed solution for 5 h , rinsed with deionized water after being taken out, and dried in an oven at 120 °C for 3 h.
[0028] A small amount of PVA was dissolved in water under the condition of heating and stirring at 80 °C to prepare a 1 wt% mass concentration solution for later use.
[0029] Measure 1 ml of 1 mg / L graphene oxide dispersion, 20 mg of attapulgite and 105 mg of 1 wt% PVA solution at a ratio of m(GO:ATP)=1:20, mix and dilute to 15 mL, and the solution was stirred for 30 min, at which point the total mass of the membrane was 22.05 mg.
[0030] Slowly pour the solution into a suction filter bottle, filter it on the Al2O3 ceramic substrate by vacuum suction, completely drain it to form a film, take it out, put it in an oven for 2 h at 50 °C, and prepare GO / ATP / PVA (5%) Composite ...
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