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A kind of fluorite flotation collector and its preparation method and application

A collector and flotation technology, used in flotation, solid separation, etc., can solve the problem that the flotation collector is not suitable for the flotation of various minerals, the selectivity of the carboxylic acid collector is poor, and the recovery rate of fluorite flotation It can achieve the effect of improving secondary enrichment, good water-soluble dispersibility and flotation selectivity, and stable flotation index.

Active Publication Date: 2020-05-05
ZHEJIANG UNIV OF TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Therefore, the technical problem to be solved in the present invention is to overcome the low recovery rate and poor repeatability of fluorite flotation in the prior art, the content of silica in the concentrate of flotation is high, and the flotation collector is not suitable for A variety of mineral flotation, poor selectivity of carboxylic acid collectors and other defects, thereby providing a fluorite flotation collector and its preparation method and application

Method used

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  • A kind of fluorite flotation collector and its preparation method and application
  • A kind of fluorite flotation collector and its preparation method and application
  • A kind of fluorite flotation collector and its preparation method and application

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Embodiment 1

[0027] This embodiment provides a kind of flotation collector and its preparation method and application, specifically,

[0028] Described flotation collector comprises the dioctyl sulfosuccinate disodium, oleic acid and ethanol that quality is 143kg, 778kg and 79kg;

[0029] The preparation method of above-mentioned flotation collector is:

[0030] sequentially add oleic acid, dioctyl sulfosuccinate disodium and ethanol into the reaction kettle, stir thoroughly for 1 hour to obtain the collector;

[0031] see figure 1 , which is a process flow diagram for the application of collectors provided by the invention in fluorite flotation, and the specific steps are as follows:

[0032] Rough separation: Grinding 1000kg of raw ore to obtain a grinding product, the content of -200 mesh in the grinding product is 58%; adding 800g of regulator sodium carbonate, 800g of inhibitor water glass, and 1000g of collector to the grinding product Rough separation to obtain rough concentrate ...

Embodiment 2

[0036] This embodiment provides a kind of flotation collector and its preparation method and application, specifically,

[0037] Described flotation collector comprises the dioctyl sulfosuccinate disodium, oleic acid and ethanol that quality is 135kg, 760kg and 85kg;

[0038] The preparation method of above-mentioned flotation collector is:

[0039] sequentially add oleic acid, dioctyl sulfosuccinate disodium and ethanol into the reaction kettle, stir thoroughly for 1 hour to obtain the collector;

[0040] The application of the above flotation collectors in fluorite flotation is:

[0041] Rough separation: Grinding 1000kg raw ore to obtain a grinding product, the content of -200 mesh in the grinding product is 58%; adding 1200g regulator sodium carbonate, 400g inhibitor water glass, and 800g collector to the grinding product Rough separation to obtain rough concentrate and rough tailings;

[0042] Beneficiation: 7 times of beneficiation, adding collector and acidified wate...

Embodiment 3

[0045] This embodiment provides a kind of flotation collector and its preparation method and application, specifically,

[0046] Described flotation collector comprises the dioctyl sodium sulfosuccinate, oleic acid and ethanol that quality is 155kg, 790kg and 65kg;

[0047] The preparation method of above-mentioned flotation collector is:

[0048] Add oleic acid, dioctyl sodium sulfosuccinate and ethanol to the reaction kettle in turn, and stir thoroughly for 1 hour to obtain the collector;

[0049] The application of the above flotation collectors in fluorite flotation is:

[0050] Rough separation: Grinding 1000kg raw ore to obtain a grinding product, the content of -200 mesh in the grinding product is 58%; add 1000g regulator sodium carbonate, 600g inhibitor water glass, and 1500g collector to the grinding product Rough separation to obtain rough concentrate and rough tailings;

[0051] Beneficiation: 7 times of beneficiation, adding collector and acidified water glass dur...

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Abstract

The invention belongs to the technical field of mineral flotation, and concretely relates to a fluorite flotation collector, and a preparation method and an application thereof. The flotation collector includes dioctyl sulfosuccinate sodium salt, oleic acid and ethanol. The flotation collector has the advantages of strong collection ability, good water-soluble dispersibility, good flotation selectivity and stable flotation index, can improve the recovery rate of fluorite flotation, and has a good repetition effect in large-scale industrial applications. Concentrate obtained by flotation usingthe collector has a high recovery rate and a low silica content, and the grade of tailings is low. Additionally, the flotation collector also can be used to float minerals at a low temperature, can effectively avoid problems such as slurry heating, and is conducive to energy saving and emission reduction.

Description

technical field [0001] The invention belongs to the technical field of mineral flotation, and in particular relates to a fluorite flotation collector and its preparation method and application. Background technique [0002] The flotation method is a mineral processing method that selectively separates minerals based on the differences in surface physical and chemical properties. It is characterized by the selective adsorption of collectors on the surface of useful minerals, so that it selectively attaches to the air bubbles in the pulp. Then it floats up to the surface of the slurry to separate the useful minerals from the gangue. Taking fluorite as an example, as the grade of fluorite raw ore becomes lower and the intercalation of fluorite and gangue minerals becomes closer and closer, only through fine grinding can the dissociation of fluorite mineral monomers be achieved. The most effective method for the separation of fine-grained ores is flotation. [0003] Chinese pa...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B03D1/00B03D1/012B03D101/02B03D103/04
Inventor 宋英王福良金火荣陈建建
Owner ZHEJIANG UNIV OF TECH
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