Method for preparing ceramsite adsorbing material from manganese slag
A technology for adsorbing materials and manganese slag, applied in the field of preparing ceramsite adsorbent materials, can solve the problems of high processing cost, low production efficiency, insufficient resource utilization, etc., so as to solve the problem of storage yard occupation, increase adsorption effect, and improve utilization value. Effect
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Embodiment 1
[0031] 1. Weigh 1 kg of manganese slag from an electrolytic manganese company in Hunan, in which the manganese content is 3.5% (wet basis) and the sulfate radical is 1.8%. Soak in 2L mixed solution containing 0.5mol / L sodium hydroxide and 0.5mol / L sodium carbonate and stir for 2 hours, then filter.
[0032] 2. Further add 0.1kg of water glass and 0.1L of 1wt% carboxypropyl cellulose, mix evenly in a kneader, extrude to granulate, and dry at 120°C.
[0033] 3. Further calcining the dried manganese sand at 600° C. for 2 hours, and cooling to obtain the ceramsite adsorption material.
[0034] 4. Take 20L of copper-containing electroplating wastewater from an electroplating industrial park in a development zone in Hubei, the copper content is 20mg / L, pH=4.5, add 0.3kg of manganese sand, stir for 2 hours, filter, and the filtrate (drainage) detects that the copper content is 0.31mg / L , can meet emission standards.
Embodiment 2
[0036] 1. Take 5kg of manganese slag from an electrolytic manganese company in Ningxia, and dry it at 120°C. The manganese content is 8.5% (dry basis), the sulfate radical is 4.5%, and the moisture content is 38.8%.
[0037] 2. Prepare sodium carbonate alkali solution, in which sodium hydroxide is 0.4mol / L and sodium carbonate is 0.8mol / L.
[0038] 3. Weigh 2 kg of manganese slag, add 5 L of sodium carbonate alkali solution, stir for 1.5 hours, and filter.
[0039] 4. Add 0.2kg of borax and 0.1L of 1wt% carboxypropyl cellulose, mix evenly in a kneader, extrude to granulate, and dry at 120°C.
[0040] 5. Dry at 120°C, calcined at 725°C for 2 hours, and cool to obtain ceramsite adsorption material.
[0041] 6. Take 20L of pretreated copper-containing waste water from a copper company in Jiangxi, where the copper content is 53mg / L, pH=5.3, add 0.4kg of ceramsite adsorption material, stir for 2 hours, filter, and detect the copper content in the filtrate (drainage) It is 0.48mg / ...
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