Shaddock peel extract liquid magnesium oxide retarder and preparation method and application thereof
A technology of liquid magnesium oxide and grapefruit peel is applied in the field of cement-based material admixtures, which can solve the problem of magnesium oxide hydration not having an effect, and achieve the effects of low price, reducing hydration heat, and prolonging setting time.
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Embodiment 1
[0023] Example 1: Clean the pomelo peel, cut off part of the white flesh (mesocarp), so that the mass ratio of mesocarp and exocarp is 1:1, chop the processed pomelo peel and put it into alcohol with 3 times the quality Soak, extract at 25°C for 24 hours, and then filter to obtain a 100% concentrated magnesium oxide retarder. Add the retarder to water and magnesium oxide in an amount of 1% by mass of magnesium oxide, stir evenly, and make a standard test piece 1, measure the initial setting time and final setting time, and record the data in Table 1.
Embodiment 2
[0024] Example 2: Clean the pomelo peel, cut off part of the white flesh (mesocarp), so that the mass ratio of mesocarp and exocarp is 1:1, chop the processed pomelo peel and put it into alcohol with 3 times the quality Soak and extract at 25°C for 24 hours, then filter to obtain the extract, heat and concentrate at 50°C to 1 / 2 of the original volume, and obtain a magnesium oxide retarder with a concentration of 200%. Add the retarder to water and magnesium oxide in an amount of 1% by mass of magnesium oxide, stir evenly, and make a standard test piece 2, measure the initial setting time and final setting time, and record the data in Table 1.
Embodiment 3
[0025] Example 3: Clean the pomelo peel, cut off part of the white flesh (mesocarp), so that the mass ratio of mesocarp and exocarp is 1:1, chop the processed pomelo peel and put it into alcohol with 3 times the quality Soak and extract at 25°C for 24 hours, then filter to obtain the extract, heat and concentrate at 50°C to 1 / 2 of the original volume, and obtain a magnesium oxide retarder with a concentration of 200%. Add the retarder to water and magnesium oxide in an amount of 2% by mass of magnesium oxide, stir evenly, make a standard test piece, measure the initial setting time and final setting time, and record the data in Table 1.
[0026] Control 1: without adding pomelo peel extract, mix lightly burned magnesia and water according to the amount, measure the initial setting time and final setting time, and record the data in Table 1.
[0027] The test method of magnesium oxide setting time in the present invention is carried out with reference to the method of GB / T1346-...
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